(E)-2-(1,3-Diphenylallyl)-3,5-dimethoxyphenol

IF 0.6 Q4 CHEMISTRY, ORGANIC Molbank Pub Date : 2023-08-04 DOI:10.3390/m1709
Lara Mollà-Guerola, Alejandro Baeza
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Abstract

The synthesis of (E)-2-(1,3-diphenylallyl)-3,5-dimethoxyphenol is described by means of the reaction of 3,5-dimethoxyphenol with (E)-1,3-diphenylprop-2-en-1-ol in 1,1,1,3,3,3-hexafluoroispropanol (HFIP), which acts as a solvent and reaction promoter. The reaction proceeds smoothly to afford the mentioned compound in high yield under a metal and additive-free procedure. The corresponding allylated phenol has been fully characterized.
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(E) -2-(1,3-二苯基烯丙基)-3,5-二甲氧基苯酚
采用3,5-二甲氧基苯酚与(E)-1,3-二苯基丙-2-烯-1-醇在1,1,1,3,3-六氟异丙醇(HFIP)中的反应,合成了(E)-2-(1,3-二苯基烯丙基)-3,5-二甲氧基苯酚。反应顺利进行,在不含金属和添加剂的程序下以高产率得到上述化合物。相应的烯丙基苯酚已经得到了充分的表征。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Molbank
Molbank Chemistry-Physical and Theoretical Chemistry
CiteScore
0.70
自引率
33.30%
发文量
174
审稿时长
11 weeks
期刊介绍: •organic synthesis •biosynthesis •extraction and purification •natural product derivatives •structural elucidation (X-ray crystallography, NMR, etc.)
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