RICE STRAW AND HUSK OIL SLUDGE FOR PROCESSING THROUGH THE USE OF LIGNOSULFONATE AS A BINDER WITH ACTIVATED CHARCOAL

N. Appazov, B. Diyarova, B. Bazarbayev, T. Assylbekkyzy, S. A. Kanzhar, B. Dzhiembaev
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Abstract

This article examines the effect of lignosulfonate binding of rice waste to oil waste to obtain activated carbon. Lignosulfonate was added to the mixture to produce briquetted activated carbon by processing rice residue (husk and straw) and oil sludge together. The mixture was carbonized and activated in a BR-12 NFT series high-temperature vacuum tube furnace with a length of 300 mm and a diameter of 60 mm and a heating section length of 200 mm in a quartz glass tube. Briquettes obtained by adding rice waste (husks and straw), oil sludge and lignosulfonate were placed in the kiln. Carbonation was carried out at a temperature of 500°C, activation was carried out at a temperature of 850°C in a ratio of 2: 1 with water vapor. The effect of the relationship of the addition of lignosulfonate binder to rice residue and oil sludge on the product properties was studied. The optimal ratio of co-treatment of the mixture was found in the ratio of rice residue: oil sludge: lignosulfonate = 9: 1: 2 (by weight). The adsorption activity of the obtained product on iodine, the total volume of pores on water, the mass fraction of moisture, the adsorption activity on methylene blue and the bulk density were studied. Activated carbon obtained from both rice straw and rice husk has high sorption properties. According to the results of experimental studies, activated carbon obtained by adding lignosulfonate to rice straw and oil sludge in a ratio of 9: 1: 2 corresponds to the brands BAС-A, WAC, BAC-Au.
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木质素磺酸盐与活性炭结合加工稻草和稻壳油泥
本文考察了木质素磺酸盐与废米油结合制备活性炭的效果。在混合料中加入木质素磺酸盐,将米渣(稻壳和秸秆)与油泥一起处理,制成压块活性炭。在长300mm、直径60mm、加热段长200mm的BR-12型NFT系列高温真空管炉中进行炭化活化。将稻糠(稻壳和秸秆)、油泥和木质素磺酸盐加入窑中制成的型煤。在500℃的温度下进行碳化,在850℃的温度下与水蒸气以2:1的比例进行活化。研究了木质素磺酸盐粘结剂在米渣和油泥中添加的关系对产品性能的影响。最佳共处理比例为米渣:油泥:木质素磺酸盐= 9:1:2(重量比)。考察了所得产物对碘的吸附活性、对水的孔隙总量、水分的质量分数、对亚甲基蓝的吸附活性和容重。从稻秆和稻壳中提取的活性炭具有较高的吸附性能。实验研究结果表明,在稻秆和油泥中以9:1:2的比例添加木质素磺酸盐得到的活性炭对应的牌号为BAС-A、WAC、BAC-Au。
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