Use of Laser Interferometry to Determine the End Time of the Plasma-Chemical Etching of p-GaN and AlGaN Layers of the p-GaN/AlGaN/GaN Heterostructure with Two-Dimensional Electron Gas

A. Yunik, A. H. Shydlouski
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Abstract

Regularities of the reflected signal intensity changing in time, recorded by the detector of the laser interferometer with the operating frequency of 670 nm during the inductively coupled plasma reactive ion etching in a Cl2/N2/O2 atmosphere of GaN, p-GaN and AlGaN in AlGaN/GaN and p-GaN/AlGaN/GaN heterostructures has been established by laser interferometry and scanning electron microscopy methods due to the changes in refractive indices and etching rates. During inductively coupled plasma reactive ion etching of GaN and p-GaN layers, the intensity of the reflected signal changes according to a periodic law with the thickness change period of about 144 nm, and for AlGaN layers about 148 nm, which is due to differences in their refractive indices and etching rates. During the crossing of the p-GaN/AlGaN and AlGaN/GaN interface, there is an abrupt change in the intensity of the reflected signal within 2.7–9.5 % for 20–40 s, due to changes in the aluminum concentration, refractive indices, and etching rate at the interfaces. The change in the periodicity of the interferogram, which is accompanied by a jump in intensity when passing through the etching front through the p-GaN/AlGaN and AlGaN/GaN interface, makes it possible to determine the end time of the inductively coupled plasma reactive ion etching of the AlGaN and p-GaN layers using laser interferometry in real time in AlGaN/GaN and p-GaN/AlGaN/GaN heterostructures with two-dimensional electron gas. The obtained results can be used to form microwave and power electronics devices elements which are based on the AlGaN/GaN heterostructures.
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用激光干涉法确定二维电子气等离子体化学刻蚀p-GaN/AlGaN/GaN异质结构p-GaN和AlGaN层的结束时间
利用激光干涉测量法和扫描电镜法,研究了在Cl2/N2/O2气氛下,在AlGaN/GaN和p-GaN/AlGaN/GaN异质结构中,GaN、p-GaN和AlGaN的电感耦合等离子体反应离子蚀刻过程中折射率和蚀刻速率的变化,建立了工作频率为670 nm的激光干涉仪探测器记录的反射信号强度随时间变化的规律。在GaN和p-GaN层的电感耦合等离子体反应离子刻蚀过程中,反射信号强度呈周期性变化,其厚度变化周期约为144 nm, AlGaN层的厚度变化周期约为148 nm,这是由于其折射率和刻蚀速率的差异造成的。在p-GaN/AlGaN和AlGaN/GaN界面交叉过程中,由于界面上铝浓度、折射率和蚀刻速率的变化,反射信号的强度在2.7 ~ 9.5%之间发生突变,持续时间为20 ~ 40 s。当通过p-GaN/AlGaN和AlGaN/GaN界面的蚀刻前沿时,干涉图的周期性变化伴随着强度的跳变,使得利用激光干涉测量技术在二维电子气体中实时测定AlGaN/GaN和p-GaN/AlGaN/GaN异质结构中AlGaN和p-GaN层的感应耦合等离子体反应离子蚀刻结束时间成为可能。所得结果可用于制备基于AlGaN/GaN异质结构的微波和电力电子器件元件。
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