A new polymorphic form of Na2SeO3·5H2O: structure determination from X-ray laboratory powder diffraction

IF 0.3 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Powder Diffraction Pub Date : 2023-08-03 DOI:10.1017/s0885715623000301
G. Nénert
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引用次数: 0

Abstract

A new polymorphic form of sodium selenite pentahydrate is reported in this contribution. We determined its crystal structure from laboratory powder diffraction data recorded at room temperature. It crystallizes in the monoclinic system P21/n with Z = 4. The lattice parameters are a = 15.01473(16) Å, b = 7.03125(7) Å, c = 8.13336(10) Å, β = 98.4458(10)°, and V = 849.345(16) Å3. The crystal structure exhibits a layered structure with isolated 1D chains running along the b-axis.
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Na2SeO3·5H2O新晶型:x射线实验室粉末衍射法的结构测定
本文报道了一种新的亚硒酸钠五水合物的多晶型。我们根据室温下记录的实验室粉末衍射数据确定了它的晶体结构。它在Z=4的单斜晶系P21/n中结晶。晶格参数为a=15.01473(16)Å,b=7.03125(7)Å、c=8.13336(10)Å和β=98.4458(10)°,以及V=849.345(16)å3。晶体结构呈现出具有沿着b轴延伸的孤立1D链的层状结构。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Powder Diffraction
Powder Diffraction 工程技术-材料科学:表征与测试
CiteScore
0.90
自引率
0.00%
发文量
50
审稿时长
>12 weeks
期刊介绍: Powder Diffraction is a quarterly journal publishing articles, both experimental and theoretical, on the use of powder diffraction and related techniques for the characterization of crystalline materials. It is published by Cambridge University Press (CUP) for the International Centre for Diffraction Data (ICDD).
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