{"title":"Developments in sample environment for a scanning transmission X-ray microscope at UVSOR-III synchrotron","authors":"Takuji Ohigashi , Nobuhiro Kosugi","doi":"10.1016/j.elspec.2023.147356","DOIUrl":null,"url":null,"abstract":"<div><p><span>The beamline, BL4U, in UVSOR-III </span>Synchrotron<span> is dedicated to scanning transmission X-ray microscopy (STXM) based on 2-dimensional soft X-ray absorption and has been in operation since 2013, to enable both academic and industrial users to carry out advanced chemical analysis under various sample environments. In this paper, we have summarized our major developments for the last decade; especially, expansion of the photon energy range down to the Li K-edge (55 eV), sample cryo-cooling to reduce radiation damage, 3-dimensional computer tomography, and air-free sample transfer.</span></p></div>","PeriodicalId":15726,"journal":{"name":"Journal of Electron Spectroscopy and Related Phenomena","volume":"266 ","pages":"Article 147356"},"PeriodicalIF":1.8000,"publicationDate":"2023-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Electron Spectroscopy and Related Phenomena","FirstCategoryId":"101","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0368204823000737","RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"SPECTROSCOPY","Score":null,"Total":0}
引用次数: 1
Abstract
The beamline, BL4U, in UVSOR-III Synchrotron is dedicated to scanning transmission X-ray microscopy (STXM) based on 2-dimensional soft X-ray absorption and has been in operation since 2013, to enable both academic and industrial users to carry out advanced chemical analysis under various sample environments. In this paper, we have summarized our major developments for the last decade; especially, expansion of the photon energy range down to the Li K-edge (55 eV), sample cryo-cooling to reduce radiation damage, 3-dimensional computer tomography, and air-free sample transfer.
期刊介绍：
The Journal of Electron Spectroscopy and Related Phenomena publishes experimental, theoretical and applied work in the field of electron spectroscopy and electronic structure, involving techniques which use high energy photons (>10 eV) or electrons as probes or detected particles in the investigation.
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