Jatropha integerrima flower extract mediated green synthesis of silver nanoparticles: spectroscopic, catalytic, and antioxidant analysis

IF 1.1 4区 化学 Q3 SPECTROSCOPY Spectroscopy Letters Pub Date : 2022-10-25 DOI:10.1080/00387010.2022.2137200
A. Bala, G. Rani, R. Ahlawat
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引用次数: 3

Abstract

Abstract Plant extract mediated nanoparticles have gained enormous attention for their green and rational approach and developed as an alternative to conventional chemical and physical methods. Here, the less exploited Jatropha integerrima flower extract is used in the synthesis of silver nanoparticles. The as-prepared nanoparticles exhibit a strong surface plasma resonance around 420 nm. Several spectroscopic techniques confirmed the formation of silver nanoparticles with an average size of 32.07 nm, stabilized by functional groups. The catalytic activity of synthesized nanoparticles for Rhodamine B dye degradation in the presence of sodium borohydride was investigated. The results showed that the 100 µL catalyst dose degraded the alkaline solution of dye up to 98%, with a high rate constant of 1.2110 min−1. In addition, the nanoparticles were tested for antioxidant activity using the 2,2-dipehnyl-1-picrylhydrazyl free radical assay. The calculated IC50 value for synthesized nanoparticles was 33.63 ± 0.53 µg/mL. Thus, the as-prepared nanoparticles are excellent candidates for catalytic and antioxidant activities compared to other materials used so far.
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麻风树花提取物介导的银纳米颗粒的绿色合成:光谱、催化和抗氧化分析
摘要植物提取物介导的纳米颗粒以其绿色、合理的方法获得了广泛的关注,并作为传统化学和物理方法的替代品而发展起来。在这里,较少开发的麻疯树花提取物被用于合成银纳米粒子。制备的纳米颗粒在420 nm附近表现出强烈的表面等离子体共振。几种光谱技术证实了银纳米颗粒的形成,其平均尺寸为32.07 nm,由官能团稳定。研究了合成的纳米颗粒在硼氢化钠存在下对罗丹明B染料降解的催化活性。结果表明,100µL催化剂对染料碱性溶液的降解率可达98%,降解速率常数为1.2110 min−1。此外,采用2,2-二苯基-1-苦味酰肼自由基法检测纳米颗粒的抗氧化活性。合成纳米颗粒的IC50值为33.63±0.53µg/mL。因此,与目前使用的其他材料相比,制备的纳米颗粒具有良好的催化和抗氧化活性。
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来源期刊
Spectroscopy Letters
Spectroscopy Letters 物理-光谱学
CiteScore
2.90
自引率
5.90%
发文量
50
审稿时长
1.3 months
期刊介绍: Spectroscopy Letters provides vital coverage of all types of spectroscopy across all the disciplines where they are used—including novel work in fundamental spectroscopy, applications, diagnostics and instrumentation. The audience is intended to be all practicing spectroscopists across all scientific (and some engineering) disciplines, including: physics, chemistry, biology, instrumentation science, and pharmaceutical science.
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