Composition optimization of PLA/PPC/HNT nanocomposites for mandibular fixation plate using single-factor experimental design.

I. Haneef, Y. Buys, N. Shaffiar, A. A. Abdul Hamid, S. I. S. Shaharuddin, Fitriani
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引用次数: 1

Abstract

The need to overcome the secondary surgery to remove implanted metal fixation plate leads to the idea of replacing the material with degradable bionanocomposite. In this research, polylactic acid/polypropylene (PLA/PPC) blends incorporated with halloysite nanotubes (HNT) (0-6 wt %) were considered as the candidate material for mandibular fixation plate. A single-factor design using Design Expert software was used to determine 20 different compositions of PLA/PPC/HNT nanocomposites and their mechanical properties were then measured. The optimization of the PLA/PPC/HNT nanocomposite composition was performed based on the nanocomposite's response to Young's modulus, tensile strength, and elongation at break. Further analysis suggested an optimum composition of 92.5/7.5 PLA/PPC with 6 wt % of HNT. The statistical results predicted that there was a 71.7% possibility that the proposed nanocomposite would have the following mechanical properties: Young's modulus of 2.18 GPa, a tensile strength of 64.16 MPa, and an elongation at break of 106.53%.
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单因素实验设计优化PLA/PPC/HNT纳米复合材料下颌骨固定板的组成。
由于需要克服移除植入金属固定板的二次手术,因此产生了用可降解生物纳米复合材料代替材料的想法。在本研究中,聚乳酸/聚丙烯(PLA/PPC)共混物加入高岭土纳米管(HNT) (0-6 wt %)被认为是下颌固定板的候选材料。采用design Expert软件进行单因素设计,确定了20种不同组成的PLA/PPC/HNT纳米复合材料的力学性能。基于纳米复合材料对杨氏模量、拉伸强度和断裂伸长率的响应,对PLA/PPC/HNT纳米复合材料进行了优化。进一步分析表明,最佳配比为92.5/7.5 PLA/PPC, HNT质量分数为6wt %。统计结果预测,该纳米复合材料具有以下力学性能的可能性为71.7%:杨氏模量为2.18 GPa,抗拉强度为64.16 MPa,断裂伸长率为106.53%。
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