Effect of Sn doping on structural, magnetic and power loss properties of lithium ferrites for high frequency applications

Q2 Physics and Astronomy Physics Open Pub Date : 2023-07-01 DOI:10.1016/j.physo.2023.100155
Neelam Singh , Manish Kumar Kansal , Praduman Kumar , Samiksha Dabas , Vivek Verma
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Abstract

The role of Sn doping on the structural, magnetic and power loss properties of Li0.5+0.5xSnxFe2.5-1.5xO4 ferrites (x = 0.0 to 0.20 in step of 0.05) + 0.5 wt % Bi2O3, prepared by solid state technique, has been investigated. X-ray diffraction reveals that Sn ions doped in lithium ferrite up to small concentration. Surface morphology recorded by SEM micrographs illustrates uniform, well connected grain growth in all samples. A small concentration of Sn doping in lithium ferrite improves the grain growth and densification. Magnetic parameters have been evaluated by M − H curves measured at room temperature by VSM. Saturation magnetization was found to be decreasing with Sn concentration in Li0.5+0.5xSnxFe2.5-1.5xO4 ferrites. In view of applicability of prepared samples for power devices, the magnetic permeability (μ* = μ′-jμ'′) has been recorded in the frequency range of 1 MHz–103 MHz at room temperature. Further, Power loss response has also been recorded in presence of magnetic induction (B = 10 mT) in frequency range of 50 kHz to 3 MHz. It was depicted a significant reduction in power loss in Sn = 0.05 doped lithium ferrite sample. Reduction in power loss with Sn doping makes it suitable for power applications.

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锡掺杂对高频应用锂铁氧体结构、磁性和功率损耗性能的影响
研究了Sn掺杂对固态法制备Li0.5+0.5 xsnxfe2.5 -1.5 xo4 (x = 0.0 ~ 0.20,步进0.05)+0.5 wt % Bi2O3铁氧体结构、磁性和功耗的影响。x射线衍射表明,铁酸锂中Sn离子的掺杂浓度很小。SEM显微照片记录的表面形貌表明,所有样品的晶粒生长均匀,连接良好。在铁酸锂中掺入少量的锡有利于晶粒的生长和致密化。磁性参数用VSM在室温下测得的M - H曲线来评价。Li0.5+0.5 xsnxfe2.5 ~ 1.5 xo4铁氧体的饱和磁化强度随Sn浓度的增加而降低。考虑到制备的样品适用于功率器件,在室温下,在1 MHz - 103 MHz的频率范围内记录了磁导率(μ* = μ' -jμ ")。此外,在50 kHz至3 MHz的频率范围内,还记录了磁感应(B = 10 mT)存在时的功率损耗响应。结果表明,Sn = 0.05掺杂铁酸锂样品的功率损耗显著降低。锡掺杂降低了功率损耗,使其适合于功率应用。
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来源期刊
Physics Open
Physics Open Physics and Astronomy-Physics and Astronomy (all)
CiteScore
3.20
自引率
0.00%
发文量
19
审稿时长
9 weeks
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