Extraction from Amber Raw Materials under Electric Spark Action

IF 1.1 Q4 ELECTROCHEMISTRY Surface Engineering and Applied Electrochemistry Pub Date : 2022-08-29 DOI:10.3103/S1068375522040044
V. Chornyi, S. Petrichenko, T. Mysiura, N. Popova,  V. L. Zavialov
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Abstract

The paper presents the results of extraction from amber, which was subjected to high-voltage electric pulse treatment in order to intensify the extraction of target components. This method of processing made it possible to achieve a high degree of grinding of the material and the occurrence of additional micro- and macropores, which increased a total contact area of the phases required for an effective process of extracting raw materials. The processing was carried out in chambers of a high-voltage pulse-periodic generator with storage capacities of 0.25 and 1.0 μF, an output voltage of 50 kV, and different number of pulses for the corresponding capacitance. Amber stones with an average size of 8.2 mm were selected for research. The process was carried out in an alcoholic medium with different electrical characteristics. The dependences of variations in the dry matter content, total mineralization, content of organic acids, active acidity pH, and optical density in the extract on the number of discharges at different pulse energies were obtained as a result. The density of amber before and after processing was determined, which showed the ability of electric spark discharges to create additional porosity of the material necessary to ensure effective internal mass transfer. The results of the study can be used for the industrial implementation of electrospark processing of amber in order to obtain extracts with a complex of useful substances applicable in food, pharmaceutical, and cosmetic industries.

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电火花作用下琥珀原料的提取
本文介绍了用高压电脉冲法对琥珀进行提取,以加强对目标成分的提取。这种加工方法可以实现对材料的高度研磨,并产生额外的微孔和大孔,这增加了有效提取原材料所需的相的总接触面积。在存储容量分别为0.25和1.0 μF、输出电压为50 kV、不同脉冲数对应电容的高压脉冲周期发生器的腔室中进行处理。选择平均尺寸为8.2 mm的琥珀石进行研究。该过程在具有不同电特性的酒精介质中进行。得到了不同脉冲能量下放电次数对提取液中干物质含量、总矿化、有机酸含量、活性酸度pH和光密度的影响。测定了加工前后琥珀的密度,这表明电火花放电能够使材料产生额外的孔隙,以确保有效的内部传质。该研究结果可用于琥珀电火花加工的工业实施,以获得具有复合有用物质的提取物,适用于食品,制药和化妆品行业。
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来源期刊
Surface Engineering and Applied Electrochemistry
Surface Engineering and Applied Electrochemistry Engineering-Industrial and Manufacturing Engineering
CiteScore
1.70
自引率
22.20%
发文量
54
审稿时长
6 months
期刊介绍: Surface Engineering and Applied Electrochemistry is a journal that publishes original and review articles on theory and applications of electroerosion and electrochemical methods for the treatment of materials; physical and chemical methods for the preparation of macro-, micro-, and nanomaterials and their properties; electrical processes in engineering, chemistry, and methods for the processing of biological products and food; and application electromagnetic fields in biological systems.
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