Special techniques for metallographic examination of irradiated fuel pin wire wrap material from EBR-II

Alan Wolfenden
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Abstract

Metallographic techniques have been developed for examination of wire wrap sections of neutron irradiated AISI 316 stainless steel from EBR-II. The special etching techniques used for metallographic examination of radiation and thermally induced precipitates, including sigma or chi phases and alpha ferrite, are documented. A description is given of the preparation of standard 3 mm dia TEM foils using a nickel plating technique to increase the effective size of the original 1.1–1.4 mm dia wires.

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EBR-II辐照燃料引脚线包材料金相检验的特殊技术
采用金相技术对EBR-II型aisi316不锈钢的中子辐照包丝截面进行了检验。特殊的蚀刻技术用于金相检查的辐射和热诱发的沉淀,包括sigma或chi相和α铁氧体,记录。描述了用镀镍技术制备标准直径3mm的TEM箔,以增加原始1.1-1.4 mm直径电线的有效尺寸。
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