Microstructure and Superconducting Properties of V-Based Laves Phase Compound Multifilamentary Wires Synthesized by a Rapidly Heating and Quenching Process to Hf-Zr/V Composite

Y. Hishinuma, A. Kikuchi, Y. Iijima, Y. Yoshida, T. Takeuchi, Kiyoshi Inoue, A. Nishimura
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引用次数: 1

Abstract

We have tried to study low activation superconducting materials of the many V‐based compound superconductors, and selected the V based Laves phase (V2(Hf,Zr)) compound because of its high upper critical field (Hc2) exceeding 20 T, its neutron irradiation resistance, and its low activation in the fusion reactor compared with those of Nb‐based A15 wires.The fabrication, microstructure and superconductivity of V2(Hf,Zr) multifilamentary wire synthesized by applying a rapidly‐heating/quenching (RHQ) and annealing process to the simple precursor using pure Hf and Zr mixture powder and pure V tube matrix were investigated. We found that a thick reaction layer was formed between the powder mixture filament and V matrix after the RHQ treatment and then it was increased with an increment of heating energy. Offset Tc values of samples were raised by increasing heating energy, and maximum Tc values occurred at 8.3 K. The maximum Jc value was obtained for a sample of post‐annealing at 600°C for 10 h. Jc dependence on...
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快速加热淬火制备Hf-Zr/V复合材料V基laaves相复合多丝丝的组织与超导性能
我们尝试研究了许多V基化合物超导体的低活化超导材料,并选择了V基Laves相(V2(Hf,Zr))化合物,因为它的上临界场(Hc2)超过20 T,耐中子辐照,并且与Nb基A15导线相比,它在聚变反应堆中的活化率低。研究了以纯Hf和Zr混合粉末和纯V管为基体,采用快速加热/淬火(RHQ)和退火工艺合成的V2(Hf,Zr)多丝的制备工艺、微观结构和超导性。我们发现,经过RHQ处理后,粉末混合灯丝与V基之间形成了一层较厚的反应层,随着加热能量的增加,反应层逐渐增大。随着加热能量的增加,样品的偏移Tc值升高,在8.3 K时达到最大值。在600°C下退火10 h后获得了最大的Jc值。
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