Synthesis of Peracetylated β-D-Glucopyranosyl Thioureas from Substituted 2-Aminobenzo-1ʹ, 3ʹ-thiazoles

N. Thanh
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引用次数: 1

Abstract

Some peracetylated glucopyranosyl thioureas containing a heterocyclic ring system, benzo-1,3-thiazole have been prepared by the condensation reaction of tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate and corresponding substituted 2-amino-(6-substituted)benzo-1,3-thiazoles. Investigated heating conditions showed that the solventless microwave-assisted method gave higher yields of these thioureas.
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取代2-氨基苯-1′,3′-噻唑合成过乙酰化β- d -葡萄糖吡喃基硫脲
以4 - o-乙酰基-β- d -葡萄糖吡喃基异硫氰酸酯与相应的2-氨基-(6-取代)苯并-1,3-噻唑为缩合反应,制备了含有杂环体系-苯并-1,3-噻唑的过乙酰化葡萄糖吡喃基硫脲。对加热条件的研究表明,无溶剂微波辅助法制备这些硫脲的收率较高。
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来源期刊
E-journal of Chemistry
E-journal of Chemistry CHEMISTRY, MULTIDISCIPLINARY-
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