{"title":"A Kind of Synthesis and Analysis of Thiazophos with High Purity","authors":"贺 李","doi":"10.12677/hjcet.2023.134030","DOIUrl":null,"url":null,"abstract":"[Aims] A novel experimental scheme for the synthesis of thiazole phosphorus was proposed. [Method] Thiazolidinone (1,3-thiazolidinone-2-one) and phosphoryl chloride (s-sec-butyl-o-ethyl thio-phosphoryl chloride) were used as raw materials. In toluene solution, supported by sodium hydride and catalyst, thiazolidinophos ((RS)-s-sec-butyl-o-ethyl-2-oxo-1, 3-thiazolidinyl-3-thioxanthate) was","PeriodicalId":61591,"journal":{"name":"化学工程与技术","volume":"1 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"化学工程与技术","FirstCategoryId":"1087","ListUrlMain":"https://doi.org/10.12677/hjcet.2023.134030","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
[Aims] A novel experimental scheme for the synthesis of thiazole phosphorus was proposed. [Method] Thiazolidinone (1,3-thiazolidinone-2-one) and phosphoryl chloride (s-sec-butyl-o-ethyl thio-phosphoryl chloride) were used as raw materials. In toluene solution, supported by sodium hydride and catalyst, thiazolidinophos ((RS)-s-sec-butyl-o-ethyl-2-oxo-1, 3-thiazolidinyl-3-thioxanthate) was
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