Manufacturing of the stainless-steel sheathed magnesium diboride superconductor wire

IF 1.4 4区 材料科学 Q3 MATERIALS SCIENCE, CERAMICS Science of Sintering Pub Date : 2023-01-01 DOI:10.2298/sos230505047y
S. Yudanto, Ahmad Affandi, Azwar Manaf
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Abstract

The Powder in Tube (PIT) method was utilized to manufacture the MgB2-based monofilament wire. The ground powders of Mg and B were filled in the stainless-steel tube and went through a cold-rolling process. In order to avoid oxidation, the wire was cut and packed into the stainless-steel tube before sintering at various temperatures (873 K, 973 K, and 1073 K). We offer this heating process in a tube as a method that was both practical and efficient. The formation of the MgB2 phase was analyzed using an X-ray diffractometer post-sintering. At the sintering temperature of 973 K, the MgB2 phase was formed which contained small amounts of magnesium oxide. The sample sintered at 973 K showed superconducting properties, with a critical temperature zero (Tc-zero) and onset (Tc-onset) of 34.09 K and 41.33 K, respectively. A large gap between Tc-onset and Tc-zero was indicated by the insufficient fraction of the MgB2 phase that formed. However, MgB2-based superconducting wire was successfully manufactured in the required tube utilizing a vacuum-free heating process and only a small amount of magnesium oxide.
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不锈钢护套二硼化镁超导体线的制造
采用管内粉末法制备了mgb2基单丝。将磨碎的Mg和B粉末填充到不锈钢管中,进行冷轧加工。为了避免氧化,在不同温度(873 K, 973 K和1073 K)烧结之前,将线材切割并装入不锈钢管中。我们提供的这种管内加热过程既实用又高效。烧结后用x射线衍射仪分析了MgB2相的形成。在973 K的烧结温度下,形成了含有少量氧化镁的MgB2相。在973 K下烧结的样品表现出超导性能,临界温度为34.09 K,起始温度为41.33 K。形成的MgB2相的比例不足表明tc开始和tc零之间存在很大的差距。然而,利用真空加热过程和少量氧化镁,在所需的管中成功地制造了基于mgb2的超导线。
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来源期刊
Science of Sintering
Science of Sintering 工程技术-材料科学:硅酸盐
CiteScore
2.50
自引率
46.70%
发文量
20
审稿时长
3.3 months
期刊介绍: Science of Sintering is a unique journal in the field of science and technology of sintering. Science of Sintering publishes papers on all aspects of theoretical and experimental studies, which can contribute to the better understanding of the behavior of powders and similar materials during consolidation processes. Emphasis is laid on those aspects of the science of materials that are concerned with the thermodynamics, kinetics and mechanism of sintering and related processes. In accordance with the significance of disperse materials for the sintering technology, papers dealing with the question of ultradisperse powders, tribochemical activation and catalysis are also published. Science of Sintering journal is published four times a year. Types of contribution: Original research papers, Review articles, Letters to Editor, Book reviews.
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