Surface morphological characterization of rf-magnetron sputtering developed inconel coated titanium

Q2 Materials Science Engineering Solid Mechanics Pub Date : 2023-01-01 DOI:10.5267/j.esm.2023.7.005
K. Babaremu, T. Jen, O. Oladijo, E. Akinlabi
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引用次数: 0

Abstract

The interconnected usefulness of titanium grade 5 is amplified by the improved mechanical ability and sustainable applications in various industries like the aerospace, medical industry and many more. Despite the profound properties of Ti6Al4V, it is worthy of intellectual study to investigate the possible performance improvement of the material for better operational application. This study adopted the use of RF magnetron sputtering to deposit the target on the substrate material under varying temperatures and deposition power. A total of four samples and control were analyzed for a surface morphological examination and post-sputtering chemical compositional analysis via SEM (scanning electron microscope) and EDX (energy dispersive x-ray analysis). Further investigation on the samples' crystallites was done using XRD (X-ray diffractometer). The SEM images showed low agglomeration and most of the samples were void of pores, cleft and crevices, which implied homogeneous distribution of the target (Inconel thin film) on the titanium substrate. The EDX of the Inconel coated titanium samples revealed elements such as Ti, Si and C, which are beneficial to the properties of the materials. The XRD profiles of the Inconel coated titanium samples disclosed intensities of high peaks, which indicated stability, chemical and microstructural homogeneity of the thin film.
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磁控溅射制备铬镍铁合金涂层钛的表面形貌表征
5级钛的相互关联的有用性被提高的机械能力和在航空航天,医疗行业等各个行业的可持续应用所放大。尽管Ti6Al4V具有深刻的特性,但为了更好的操作应用,探索材料可能的性能改进是值得智力研究的。本研究采用射频磁控溅射技术,在不同温度和沉积功率下将靶材沉积在衬底材料上。通过扫描电镜(SEM)和能量色散x射线分析(EDX)对4个样品和对照进行表面形貌检查和溅射后化学成分分析。利用x射线衍射仪(XRD)对样品的晶体进行了进一步的研究。扫描电镜结果显示,靶材(Inconel薄膜)在钛基体上分布均匀,团聚现象较弱,且大部分样品中没有孔隙、裂缝和缝隙。涂层钛样品的EDX显示了有利于材料性能的Ti、Si和C等元素。经铬镍铁合金包覆的钛样品的XRD谱显示出较高的峰强度,表明薄膜的稳定性、化学性质和微观结构均匀。
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来源期刊
Engineering Solid Mechanics
Engineering Solid Mechanics Materials Science-Metals and Alloys
CiteScore
3.00
自引率
0.00%
发文量
21
期刊介绍: Engineering Solid Mechanics (ESM) is an online international journal for publishing high quality peer reviewed papers in the field of theoretical and applied solid mechanics. The primary focus is to exchange ideas about investigating behavior and properties of engineering materials (such as metals, composites, ceramics, polymers, FGMs, rocks and concretes, asphalt mixtures, bio and nano materials) and their mechanical characterization (including strength and deformation behavior, fatigue and fracture, stress measurements, etc.) through experimental, theoretical and numerical research studies. Researchers and practitioners (from deferent areas such as mechanical and manufacturing, aerospace, railway, bio-mechanics, civil and mining, materials and metallurgy, oil, gas and petroleum industries, pipeline, marine and offshore sectors) are encouraged to submit their original, unpublished contributions.
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