Effect of Titanium Dioxide Nano Particles Incorporation on Mechanical and Physical Properties on Two Different Types of Acrylic Resin Denture Base

Mohamed Ahmed, M. El-Shennawy, Yousef M. Althomali, A. Omar
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引用次数: 69

Abstract

The aim of this study is to clarify the effect of different concentrations of titanium dioxide nanoparticles (Nps) on the properties of two types of heat polymerized acrylic resin. The tested parameters were flexural strength, impact strength, and microhardness. The two types of acrylic resin used in this study were conventional unmodified (Implacryl, Vertex) and high impact heat polymerized acrylic resin (Vertex-Dental, Netherlands). Both types of acrylic resin were modified by using 1% and 5% TiO2 Nps powder. Specimen’s dimensions were prepared according to the American Dental Association Specification No. 12. Three types of specimens were prepared: 1) flexural strength specimens 50 mm × 10 (±0.2) mm × 3 (±0.2) mm, 2) impact strength test specimens 60 mm × 6.0 mm × 4.0 mm, 3) microhardnesss specimens 25 mm × 10 mm × 3 (±0.2) mm. For each test 6 groups were prepared (each group containing 5 samples). Thirty specimens were prepared in each of the three tests, amounting to a total number of 90 specimens. Mechanical properties such as flexural strength (FS), impact strength and microhardness of the above mentioned specimens were determined using universal testing machine, Izod pendulum impact testing machine and Vickers microhardness tester, respectively. ISO Specification No. 1567 was followed in microhardness test. The data was collected and statistically analyzed. Flexural strength considerably decreased by increasing TiO2 concentration in both types of acrylic resin. Impact strength of the conventional acrylic resin modified by 1% of additives significantly increased. The microhardness is significantly increased by addition of 5% of TiO2 Nps. The Incorporation of TiO2 nanoparticles into acrylic resins can adversely affect its flexural strength. Meanwhile, the impact strength can be modified by small percentage of additives (abt. 1%). This effect is directly correlated with the concentration of nanoparticles. On the other hand, concentrations of TiO2 Nps (abt. 5%) positively affect the microhardness of both types of acrylic resin used in the present study.
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纳米二氧化钛颗粒掺入对两种不同类型丙烯酸树脂义齿基托力学物理性能的影响
本研究的目的是阐明不同浓度的二氧化钛纳米颗粒(Nps)对两种热聚合丙烯酸树脂性能的影响。测试参数为抗弯强度、冲击强度和显微硬度。本研究中使用的两种丙烯酸树脂是常规的未改性丙烯酸树脂(Implacryl, Vertex)和高冲击热聚合丙烯酸树脂(Vertex- dental,荷兰)。分别用1%和5%的TiO2 Nps粉末对两种丙烯酸树脂进行改性。样品的尺寸根据美国牙科协会规范第12号制备。制备三种试样:1)抗弯强度试样50 mm × 10(±0.2)mm × 3(±0.2)mm, 2)冲击强度试样60 mm × 6.0 mm × 4.0 mm, 3)显微硬度试样25 mm × 10 mm × 3(±0.2)mm,每组制备6组(每组5个试样)。三次试验各制备30个试样,共制备90个试样。采用万能试验机、伊佐德摆锤式冲击试验机和维氏显微硬度计分别测定上述试样的抗弯强度(FS)、冲击强度和显微硬度等力学性能。显微硬度试验按照ISO 1567规范进行。收集数据并进行统计分析。随着TiO2浓度的增加,两种类型的丙烯酸树脂的抗弯强度显著降低。常规丙烯酸树脂经1%的添加剂改性后,冲击强度明显提高。添加5%的TiO2 Nps可显著提高材料的显微硬度。二氧化钛纳米颗粒掺入丙烯酸树脂中会对丙烯酸树脂的抗弯强度产生不利影响。同时,加入少量的添加剂(约1%)也能提高材料的冲击强度。这种效应与纳米颗粒的浓度直接相关。另一方面,TiO2 Nps的浓度(约5%)正影响本研究中使用的两种丙烯酸树脂的显微硬度。
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