Performance of a next generation vial autosampler for the analysis of VOCs in water matrices

Ed Price
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Abstract

In today's laboratories, increased efficiency and productivity are of extreme importance. Equally important is the ability to automate analyses without sacrificing sample integrity or data quality. A new vial autosampler has been developed to fully automate purge and trap analysis of water and wastewater samples in accordance with current EPA methods for volatile analysis. Research is presented demonstrating the autosampler's ability to transfer sample aliquots with the addition of internal standard or surrogate solutions. Data are evaluated for linearity, precision, and accuracy. In addition, the instrument's sample pathway is evaluated for carryover, inertness, and reliability.

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用于分析水基质中挥发性有机物的下一代小瓶自动进样器的性能
在当今的实验室中,提高效率和生产力至关重要。同样重要的是在不牺牲样本完整性或数据质量的情况下实现分析自动化的能力。已经开发了一种新的小瓶自动进样器,以根据当前EPA的挥发性分析方法,完全自动化水和废水样品的吹扫和捕集分析。研究证明了自动进样器在添加内标或替代溶液的情况下转移等分试样的能力。对数据的线性、精度和准确性进行评估。此外,还对仪器的样本路径进行了携带、惰性和可靠性评估。
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Preface Publisher's note Data acquisition, analysis and processing Optimization of laboratory experiments Author index volume 34
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