Evaluation and Comparison of Newly Developed Phosphoric Acid Gel (Exir) with Two Different Common Gels in Iran

H. Mohammadipour, M. Akbari, H. Bagheri, M. Malekmohammadi, Elnaz Karimian, Salehe Sekandari
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Abstract

Introduction: Different surface treatments were preposed to prepare the tooth structure for resin composite bonding. One of the most common preparation is using of phosphoric acid etching. This study conducted to determine the etching effectiveness of a new formulated acid etchant (Exir) and compared it with two commercial products. Methods: To determine the physical properties, the viscosity and shelf life were evaluated by a viscometer and a centrifuge over the time, respectively. SEM micrographs were uesd to show the geometry of bovine enamel and dentin surfaces which were treated by three etchants. The µSBS of composite to treated dental tissues was also investigated. Data were analyzed by ANOVA and Tukey test (α=0.05). Results: Exir etchant showed the lower viscosity compared with two other gels and two-phase separation did not significantly increase during suggested period. The SEM images of enamel samples treated with Exir etchant showed regular etching patterns and less remnant in comparison with other groups. The SEM mages of dentin samples treated with Exir etchant, unlike others, showed wide open dentin tubules with clear exposed collagen fibers. Enamel and dentin µSBS were 30.08±6.79 and 7.29±1.27 for Exir etchant, 23.31±6.64 and 8.49±3.61 for Morva Etch and 23.22±7.05 and 6.16±1.68 for Ultra-Etch, respectivley. The µSBS values ​​for enamel was significantly higher in Exir treated group (P=0.017), while there was no significant difference in dentin µSBS values among three tested etchants (P=0.07). Conclusion: The results of this study showed Exir etchant can provide acceptable results used on dentin and enamel substrates.
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伊朗新开发的磷酸凝胶(Exir)与两种不同的普通凝胶的评价和比较
介绍:采用不同的表面处理方法制备树脂复合粘接齿结构。最常用的制备方法之一是采用磷酸蚀刻法。本文研究了一种新配制的酸蚀剂(Exir)的蚀刻效果,并与两种市售产品进行了比较。方法:测定物理性质,粘度和保质期分别通过粘度计和离心机的时间。用SEM显微照片显示了三种腐蚀剂处理过的牛牙釉质和牙本质表面的几何形状。研究了复合材料对牙组织的微SBS作用。数据采用方差分析和Tukey检验(α=0.05)。结果:与其他两种凝胶相比,Exir蚀刻剂的粘度较低,两相分离在建议时间内没有明显增加。用Exir蚀刻剂处理后的牙釉质样品的SEM图像显示出规律的蚀刻图案,与其他组相比残留较少。用Exir腐蚀剂处理的牙本质样品的扫描电镜图像显示,与其他样品不同,牙本质小管开阔,胶原纤维清晰暴露。Exir、Morva、Ultra-Etch分别为30.08±6.79、7.29±1.27、23.31±6.64、8.49±3.61、23.22±7.05、6.16±1.68。Exir处理组牙釉质的µSBS值显著升高(P=0.017),而三种腐蚀剂对牙本质的µSBS值差异无统计学意义(P=0.07)。结论:Exir蚀刻剂在牙本质和牙釉质基质上具有良好的效果。
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