Synthesis and Characterization of 10-Hexyl-10H-phenothiazine-3-carbaldehyde-4-phenylthiosemi-carbazone and 4-Methylbenzaldehyde-4-methylthiosemicarbazone

N. R. Jyothi, N. Farook
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Abstract

Two Schiff bases 10-hexyl-10H-phenothiazine-3-carbaldehyde-4-phenylthiosemicarbazone (HPCPTSC) and 4-methylbenzaldehyde-4-methylthiosemicarbazone (MBMTSC) were synthesized. Both the HPCPTSC and MBMTSC were characterized by elemental analysis, molar conductivity studies, Fourier transform infrared spectroscopy (FT-IR), nuclear magnetic resonance spectroscopy (NMR) and x-ray powder diffraction (XRD). All the spectral studies confirmed that the formation of both HPCPTSC and MBMTSC. Thermal stabilities of the both Schiff bases were reported based on thermogravimetric analysis (TGA) studies
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10-己基-10 - h -吩噻嗪-3-卡丁醛-4-苯基硫代氨基卡丁酮和4-甲基苯甲醛-4-甲基硫代氨基卡丁酮的合成与表征
合成了两个希夫碱-10 -己基-10 -h -吩噻嗪-3-乙醛-4-苯基硫代氨基脲(HPCPTSC)和4-甲基苯甲醛-4-甲基硫代氨基脲(MBMTSC)。采用元素分析、摩尔电导率、傅里叶变换红外光谱(FT-IR)、核磁共振光谱(NMR)和x射线粉末衍射(XRD)对HPCPTSC和MBMTSC进行了表征。所有的光谱研究都证实了HPCPTSC和MBMTSC的形成。基于热重分析(TGA)研究报道了这两种希夫碱的热稳定性
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