{"title":"EXTRACTION OF PHENOLIC COMPOUNDS OF ASPEN AND WILLOW LEAVES OF THE SALICACEAE FAMILY","authors":"G. R. Arslanova, D. Prosvirnikov, R. Safin","doi":"10.34220/mmeitsic2021_17-22","DOIUrl":null,"url":null,"abstract":"The paper presents the results of studies on the extraction of phenolic compounds from the leaves of trees of the Salicaceae family, namely aspen and willow. A method for extracting phenolic compounds of salicin and quercetin by extraction using ethyl alcohol as a solvent is described. The method of identification of salicin and quercetin by thin-layer chromatography (TLC) is described. Digital processing of the obtained results was carried out using the computer program “Sorbfil Visualizer” (Krasnodar). The optimal operating parameters of the process, allowing to obtain the highest yield of the desired substances, are determined. The maximum yield of quercetin in the amount of 1.4% a. s. v. was obtained from aspen leaves, and was achieved at the following extraction parameters: the concentration of the ethyl alcohol solution (extractant) – 60%, the extraction duration-30 min, the temperature of the extractant-50°C. The maximum yield of salicin from aspen leaves is 0.26% a. s. v. and is achieved at.","PeriodicalId":18702,"journal":{"name":"Modern machines, equipment and IT solutions for industrial complex: theory and practice : materials of the All-Russian scientific and practical conference, Voronezh, June 17, 2021 / ed. T.L. Ishchenko, D.A. Parinov, N.V. Truskova","volume":"22 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Modern machines, equipment and IT solutions for industrial complex: theory and practice : materials of the All-Russian scientific and practical conference, Voronezh, June 17, 2021 / ed. T.L. Ishchenko, D.A. Parinov, N.V. Truskova","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.34220/mmeitsic2021_17-22","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract

The paper presents the results of studies on the extraction of phenolic compounds from the leaves of trees of the Salicaceae family, namely aspen and willow. A method for extracting phenolic compounds of salicin and quercetin by extraction using ethyl alcohol as a solvent is described. The method of identification of salicin and quercetin by thin-layer chromatography (TLC) is described. Digital processing of the obtained results was carried out using the computer program “Sorbfil Visualizer” (Krasnodar). The optimal operating parameters of the process, allowing to obtain the highest yield of the desired substances, are determined. The maximum yield of quercetin in the amount of 1.4% a. s. v. was obtained from aspen leaves, and was achieved at the following extraction parameters: the concentration of the ethyl alcohol solution (extractant) – 60%, the extraction duration-30 min, the temperature of the extractant-50°C. The maximum yield of salicin from aspen leaves is 0.26% a. s. v. and is achieved at.
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水杨科杨树和柳树叶中酚类化合物的提取
本文介绍了从水杨科树木白杨和柳树叶片中提取酚类化合物的研究结果。介绍了一种以乙醇为溶剂提取水杨苷和槲皮素酚类化合物的方法。建立了水杨苷和槲皮素的薄层色谱鉴别方法。使用计算机程序“Sorbfil Visualizer”(Krasnodar)对所获得的结果进行数字处理。确定了该工艺的最佳操作参数,以获得所需物质的最高收率。在乙醇溶液(萃取剂)浓度为60%、萃取时间为30 min、萃取温度为50℃的条件下,槲皮素提取率最高,为1.4% a.s. v。杨树叶片中水杨苷的最高产率为0.26%。
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