Synthesis of Silver Nanoparticles by Phyllanthus emblica Plant Extract and Their Antibacterial Activity

R. Meena, Risikesh Meena, D. Arya, Sapana Jadoun, R. Hada, Roopa Kumari
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引用次数: 14

Abstract

The silver nanoparticle was successfully synthesized by using the help of Phyllanthus emblica plant extract as a reducing agent and aqueous silver nitrate as the precursor. Moreover, physical and chemical methods are widely used for the synthesis of nanoparticles, but these methods have expensive and not ecofriendly. This study highlights the green, rapid, facile, cost-effective, and ecofriendly synthesis and synthesized nanoparticles also investigate their antibacterial activity. Synthesized silver nanoparticles are analyzed by different techniques of modes like XRD, UV-Visible spectroscopy, TEM, FTIR, and photoluminescence (PL). The prepared AgNPs show characteristic absorption peak in UV-Visible spectroscopy due to SPR (surface plasmonic resonance) band between 400 to 450 nm wavelength, which was confirmed by TEM (transmission electron microscopy) image. X-ray diffraction (XRD) results showed the crystalline nature of AgNPs as well as the size of nanoparticles calculated with the help of TEM (20-25 nm) and XRD (25 nm). ATR spectroscopy identified the functional groups that are involved in the reduction of silver ion to AgNPs and the PL spectrum indicates higher emission in the green region and low emission peak in the UV region. Antibacterial activity of AgNPs analyzed against with the help of E.Coli bacteria and the result shows that a higher concentration of AgNPs is increasing as well as a zone of inhibition increased. This method is environmentally friendly, of low cost, Material Science Research India www.materialsciencejournal.org ISSN: 0973-3469, Vol.17, No.(2) 2020, Pg. 136-145 CONTACT Rajesh Kumar Meena 1988rajeshmeena@gmail.com Department of Chemistry, Kalindi College, University of Delhi, Delhi, India. © 2020 The Author(s). Published by Oriental Scientific Publishing Company This is an Open Access article licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License Doi: http://dx.doi.org/10.13005/msri/170206 Article History Received: 31 July 2020 Accepted: 26 August 2020
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余甘子提取物合成纳米银及其抑菌活性研究
以余甘子植物提取物为还原剂,硝酸银为前驱体,成功合成了纳米银颗粒。此外,物理和化学方法被广泛用于纳米颗粒的合成,但这些方法昂贵且不环保。本研究重点研究了绿色、快速、简便、经济、环保的纳米颗粒合成方法,并对其抗菌活性进行了研究。通过XRD、uv -可见光谱、TEM、FTIR、PL等不同的模式对合成的银纳米颗粒进行分析。制备的AgNPs在400 ~ 450 nm波段的紫外可见光谱中表现出特征吸收峰,透射电镜证实了这一点。x射线衍射(XRD)结果显示了AgNPs的结晶性质,并通过TEM (20 ~ 25 nm)和XRD (25 nm)计算了纳米颗粒的尺寸。ATR光谱鉴定了参与银离子还原为AgNPs的官能团,PL光谱显示绿色区发射较高,紫外区发射峰较低。利用大肠杆菌对AgNPs进行抑菌活性分析,结果表明AgNPs的抑菌浓度越来越高,抑菌区也越来越大。这种方法是环保的,低成本的,材料科学研究印度www.materialsciencejournal.org ISSN: 0973-3469, Vol.17, No.(2) 2020, Pg. 136-145联系Rajesh Kumar Meena 1988rajeshmeena@gmail.com德里大学Kalindi学院化学系,德里,印度。©2020作者。这是一篇基于知识共享署名-非商业性-相同方式共享4.0国际许可协议的开放获取文章Doi: http://dx.doi.org/10.13005/msri/170206文章历史收稿日期:2020年7月31日接受日期:2020年8月26日
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