Effect of hydrogen absorption on strain-induced low-cycle fatigue of low carbon steel

Y. Tsuchida, T. Watanabe, T. Kato, T. Seto
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引用次数: 23

Abstract

The effects of hydrogen have been studied on low carbon steel (JIS S10C), which contains limited amount of pearlite. Fatigue life and its strain rate dependence have been examined. The possible mechanism of hydrogen effect on those properties has been discussed. The hydrogen absorbed was 0.5–1.5 mass-ppm, according to the thermal desorption analysis (TDA). Main part of the hydrogen is dissolved in the matrix; the rest part is trapped by pearlite. This small hydrogen severely reduces the fatigue life, even in S10C steel that is considered to be less susceptible to hydrogen embrittlement. The more the hydrogen is absorbed, the less the fatigue life is. Hydrogen absorption also causes the increase in stress amplitude. Fractographic examination revealed the fracture process as the followings. The hydrogen gasifies at the interface between the non-metallic inclusion and matrix. Then the high pressure hydrogen gas atmosphere maintains hydrogen content in the matrix around inclusion. This assists the crack initiation at the interface of inclusion, and also assists the crack propagation through producing the fish-eye fracture. According to the published works on non-hydrogen charged specimens, vacancy plays an important role in both crack initiation and propagation, and determines the fatigue life. The stress amplitude is believed also influenced by the vacancy that is produced by the movement of jogged dislocation. When these vacancies are stabilized by hydrogen, fatigue life will be decreased with the increased stress amplitude. Fatigue life is decreased with slower strain rate test. Stress amplitude shows the negative dependence to the strain rate. These are claimed as the features of dynamic strain aging (DSA). Considering the above mentioned knowledge on vacancy stabilized by hydrogen, the DSA is brought about by the interaction between dislocation and vacancy-hydrogen pair.

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氢吸收对低碳钢应变诱导低周疲劳的影响
研究了氢对含有少量珠光体的低碳钢(JIS S10C)的影响。研究了疲劳寿命及其与应变速率的关系。讨论了氢对这些性能影响的可能机理。根据热解吸分析(TDA),氢气吸收量为0.5-1.5质量-ppm。氢的主体部分溶解在基体中;其余部分被珠光体捕获。这种小氢严重降低了疲劳寿命,即使在被认为不太容易受到氢脆影响的S10C钢中也是如此。氢吸收越多,疲劳寿命越短。吸氢也引起应力幅值的增大。断口检查显示断裂过程如下。氢气在非金属夹杂物与基体的界面处气化。然后高压氢气气氛维持包裹体周围基体中的氢含量。这有利于夹杂物界面处裂纹的萌生,也有利于裂纹的扩展,产生鱼眼断裂。对非荷氢试样的研究表明,空位在裂纹萌生和扩展过程中都起着重要作用,并决定着疲劳寿命。应力幅值也被认为受到由位错运动产生的空位的影响。当这些空位被氢稳定后,随着应力幅值的增大,疲劳寿命会降低。应变速率越慢,疲劳寿命越低。应力幅值与应变速率呈负相关。这些被称为动态应变老化(DSA)的特征。考虑到上述关于氢稳定空位的知识,DSA是位错与空位-氢对相互作用产生的。
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