Effects of Carbonization Parameters on the COD Reduction of Rhodamine B Dye Aqueous Solutions Using Elaeis guineensis Frond Fiber

Ling Wei Low, T. Teng, N. Morad, B. Azahari
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Abstract

A B S T R A C T The effects of various carbonization parameters on the COD reduction of Rhodamine B dye aqueous solutions using carbonized Elaeis guineensis frond fiber (EGFF) chars have been studied experimentally. The adsorbent with the particle size of <45 µm has been carbonized at temperature from 500-900 o C with carbonization duration of 1-3 h at a heating rate of 10-30 o C/min and nitrogen gas flow rate of 100-500 cm 3 /min. Carbonization temperature, carbonization duration, heating rate and nitrogen gas flow rate were significantly affecting the carbonization process. Statistical analysisresponse surface methodology (RSM)- face centered composite design (FCCD) was used to obtain the optimal carbonization conditions. The optimum condition for carbonization of EGFF was obtained at carbonization temperature of 899 o C, carbonization duration of 2.7 h, heating rate of 10 o C/min, and nitrogen flow rate of 243 cm3/min with 98.88 % of COD reduction of Rhodamine B
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炭化参数对荷叶纤维还原罗丹明B染料水溶液COD的影响
实验研究了不同炭化参数对炭化豚鼠叶纤维(EGFF)炭还原罗丹明B染料水溶液COD的影响。对粒径<45µm的吸附剂进行炭化,炭化温度为500 ~ 900℃,炭化时间为1 ~ 3 h,升温速率为10 ~ 30℃/min,氮气流量为100 ~ 500 cm 3 /min。炭化温度、炭化时间、升温速率和氮气流量对炭化过程有显著影响。采用统计分析、响应面法(RSM)-面心复合设计(FCCD)确定了最佳碳化条件。结果表明,EGFF的最佳炭化条件为:炭化温度899℃,炭化时间2.7 h,升温速率10℃/min,氮气流量243 cm3/min,罗丹明B的COD还原率为98.88%
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