Structural Characterization of a New Schiff-Base Ligand, 1,4-Bis-(5-methyl-4-methylenamino-2,4-dihydro-[1,2,4]triazol-3-thion)-benzene [C14H14N8S2·2C2H6OS]
{"title":"Structural Characterization of a New Schiff-Base Ligand, 1,4-Bis-(5-methyl-4-methylenamino-2,4-dihydro-[1,2,4]triazol-3-thion)-benzene [C14H14N8S2·2C2H6OS]","authors":"M. Tabatabaee, M. Ghassemzadeh, Nazanin Soleimani","doi":"10.2116/ANALSCIX.24.X173","DOIUrl":null,"url":null,"abstract":"The title compound, C14H14N8S2·2C2H6OS, crystallizes in the monoclinic space group P21/c with a = 12.866(5), b = 8.126(3), c = 11.833(4)A, β = 101.239(9)°, Z = 2, Dx = 1.409 g cm-3. In the solid states, N2-H2A…O1 and C4-H4A…S1 hydrogen bonds link 2 molecules of solvent (Me2SO) to I.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"359 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Sciences: X-ray Structure Analysis Online","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2116/ANALSCIX.24.X173","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3
Abstract
The title compound, C14H14N8S2·2C2H6OS, crystallizes in the monoclinic space group P21/c with a = 12.866(5), b = 8.126(3), c = 11.833(4)A, β = 101.239(9)°, Z = 2, Dx = 1.409 g cm-3. In the solid states, N2-H2A…O1 and C4-H4A…S1 hydrogen bonds link 2 molecules of solvent (Me2SO) to I.
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