Morphological Effect on Swelling Behaviour of Carboxymethyl Cellulose–Maleic Acid Hydrogel Modified with Kombucha Bacterial Cellulose

Tanty N. Siahaan, Basuki Basuki, Amir H. Siregar, Dede I. Muthawali
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Abstract

The incorporation of bacterial cellulose from kombucha tea in carboxymethyl cellulose / maleic acid (CMC / MA) hydrogels has been successfully conducted. This study aims to analyze the relationship between the pores on the surface of the hydrogel with their water-absorbing ability. Bacterial cellulose from kombucha (KBC) was confirmed by the spectrum of OH, C-O-C, and C-OH functional groups with FT - IR analysis. Filler KBC was added to CMC / MA hydrogel with variations in the concentration of 2, 4, 6, and 8 % wt. The CMC / MA / KBC hydrogels were characterized by swelling test, degree of crosslinking, FTIR, and SEM. The swelling results showed that hydrogels with 2 % KBC produced the best water absorbing ability up to 172 %, water absorption decreased with the increase of KBC concentrations. Furthermore, SEM image results showed that the addition of KBC affects the morphological shape and pore size of the hydrogel. Meanwhile, FTIR analysis showed that there were no major changes in the functional groups of hydrogels.
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康普茶菌纤维素改性羧甲基纤维素-马来酸水凝胶溶胀行为的形态学影响
成功地将康普茶细菌纤维素掺入羧甲基纤维素/马来酸(CMC / MA)水凝胶中。本研究旨在分析水凝胶表面孔隙与其吸水能力之间的关系。利用红外光谱(FT - IR)分析了康普茶(KBC)细菌纤维素的OH、C-O-C和C-OH官能团。将填料KBC添加到CMC / MA水凝胶中,浓度分别为2、4、6和8% wt。CMC / MA / KBC水凝胶通过膨胀试验、交联度、FTIR和SEM进行表征。溶胀结果表明,KBC浓度为2%的水凝胶吸水率最高,可达172%,吸水率随KBC浓度的增加而降低。SEM结果表明,KBC的加入影响了水凝胶的形态和孔径。同时,FTIR分析表明,水凝胶的官能团没有发生大的变化。
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