Comparing Photocatalytic Activity of ZnO and Nanospherical ZnO/Bentonite Catalyst: Preparation, Structural Characterization and their Photocatalytic Performances using Oxytetracycline Antibiotic in Aqueous Solution

A. Vaizoğullar
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引用次数: 2

Abstract

Photocatalytic degradation of Oxytetracycline (OTC) in aqueous solution was performed using pure ZnO and ZnO/Bent composites. Both catalysts were synthesized trough a simple one-step chemical precipitation method. The prepared samples were characterized using SEM-EDAX and XRD analysis. Due to the immobilization of ZnO nanospheres upon bentonite surface, 25.67 m2 g-1 of specific surface area was obtained for the ZnO/Bent which lower than the specific surface area of the raw bentonite (112.25 m2 g-1). ZnO/Bent catalyst showed the best photocatalytic performance than ZnO for OTC degradation under UV light.
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氧化锌与纳米球形氧化锌/膨润土催化剂的光催化活性比较:制备、结构表征及其在水溶液中对土霉素的光催化性能
采用纯ZnO和ZnO/Bent复合材料对水溶液中土霉素(OTC)进行光催化降解。两种催化剂均通过简单的一步化学沉淀法合成。采用SEM-EDAX和XRD对制备的样品进行了表征。由于ZnO纳米球固定在膨润土表面,ZnO/Bent的比表面积为25.67 m2 g-1,低于原料膨润土的比表面积(112.25 m2 g-1)。在紫外光下,ZnO/弯曲催化剂对OTC降解的光催化性能优于ZnO。
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