{"title":"The Template Synthesis, Characterization, and Thermal Investigation of New Heterocyclic Binucleating Schiff Base Complexes","authors":"M. Sönmez, M. Şekerci","doi":"10.1081/SIM-200026585","DOIUrl":null,"url":null,"abstract":"Abstract 1‐Amino‐5‐benzoyl‐4‐phenyl‐1H‐pyrimidine‐2‐one (L′H2) reacts with benzil (L″O2) and salts Cu(AcO)2 · H2O, NiCl2 · 6H2O, Co(AcO)2 · 4H2O, CdCl2 · 2H2O in 2:1:2 molar ratio in n‐butanol to give several solid complexes of the general composition [(M)2(L′)2(L″)(X)4] · nH2O. The precursor and the metal complexes of the Schiff base have been characterized by elemental analyses, molar conductances, IR spectra, electronic, and thermal studies.","PeriodicalId":22160,"journal":{"name":"Synthesis and Reactivity in Inorganic and Metal-organic Chemistry","volume":"95 1","pages":"1551 - 1561"},"PeriodicalIF":0.0000,"publicationDate":"2004-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"8","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Synthesis and Reactivity in Inorganic and Metal-organic Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1081/SIM-200026585","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 8
Abstract
Abstract 1‐Amino‐5‐benzoyl‐4‐phenyl‐1H‐pyrimidine‐2‐one (L′H2) reacts with benzil (L″O2) and salts Cu(AcO)2 · H2O, NiCl2 · 6H2O, Co(AcO)2 · 4H2O, CdCl2 · 2H2O in 2:1:2 molar ratio in n‐butanol to give several solid complexes of the general composition [(M)2(L′)2(L″)(X)4] · nH2O. The precursor and the metal complexes of the Schiff base have been characterized by elemental analyses, molar conductances, IR spectra, electronic, and thermal studies.
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