Application of Response Surface Methodology (RSM) for Optimizing Turbidity of Paper Recycling Wastewater Using Microwave Technology

U. Ozkan, Okan Bayram, Fethiye Göde, Sezen Coskun, H. Şahin
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引用次数: 2

Abstract

Aims: The aim of the study was to use Response Surface Methodology (RSM) to find optimal experimental design for wastewater treatments from office paper recycling.  In this way, interactive effects of treatment factors were evaluated, including microwave power (MW) and durations with centrifuge time while turbidity of wastewater was chosen as the dependent output variable or an optimal response. Methodology: The RSM approach was utilized for optimization of the process parameters and identifying the optimal conditions for the removal of turbidity in paper recycling wastewater. In this regard, a three-factor RSM were selected, using MW irradiation power (Watts), durations (seconds) and centrifuge time (min). Statistical analysis of variance (ANOVA) was carried out to identify the adequacy of the developed model.  In this case, specially prepared office papers (one-side laser printed) were subjected to standard paper recycling procedure for obtaining wastewater at laboratory conditions. The experimentally derived RSM model was validated using range of statistical parameters. Conclusions:  The study revealed that under the RSM optimized conditions, a marked                reduction in the turbidity of wastewater was observed for both groups studied. The R2, R2(adj) and R2(pred) values were indicates, the developed model was significant which revealed a well agreement between the experimental data and proposed model. In this approach, the R2=99.710% and lack-of-fit value were found to be 0.111 (p>0.05), which shows the model and the data consisted to each other.  The lowest turbidity value was found with 150.000 Watts and 60.000 seconds in MW conditions with 15.000 minutes of centrifugation time, experimentally. With employing                        these variables, the turbidity value of 6.65 NTU was determined. However, the highest turbidity value of 18.013 NTU was found with MW power of 200.00 Watts with 40.000 seconds of durations and 1.591 minute of centrifugation time.  It is important to note that with using optimized parameters, the turbidity value of 1.43 NTU was calculated while 1.47 NTU was found with experimentally.
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响应面法在微波造纸废水浊度优化中的应用
目的:利用响应面法(RSM)寻找办公用纸回收废水处理的最佳实验设计。通过这种方式,评估了处理因素的交互效应,包括微波功率(MW)和离心时间,同时选择废水的浊度作为依赖输出变量或最佳响应。方法:采用RSM法对工艺参数进行优化,确定造纸废水浊度去除的最佳条件。在这方面,我们选择了一个三因素RSM,使用MW辐照功率(Watts),持续时间(秒)和离心时间(min)。进行方差统计分析(ANOVA)以确定所开发模型的充分性。在这种情况下,特别制备的办公纸(单面激光打印)在实验室条件下进行标准的纸张回收程序,以获得废水。利用统计参数范围对实验导出的RSM模型进行了验证。结论:研究发现,在RSM优化条件下,两组废水的浊度均有显著降低。R2、R2(adj)和R2(pred)值表明,所建模型具有显著性,实验数据与所建模型吻合较好。在此方法中,发现R2=99.710%,缺乏拟合值为0.111 (p>0.05),说明模型与数据相互组成。实验发现,在150.000瓦、60000秒、MW条件下,离心时间为15000分钟,浊度值最低。利用这些变量,确定了6.65 NTU的浊度值。然而,当MW功率为200.00瓦,持续时间为40000秒,离心时间为1.591分钟时,浊度值最高,为18.013 NTU。值得注意的是,使用优化参数计算得到的浊度值为1.43 NTU,而实验结果为1.47 NTU。
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