Micro-Crack Healing in Cubic Zirconia (8Y-CSZ) Using Flash Event

Fuki Naito, K. Morita, D. Terada
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引用次数: 1

Abstract

The e ff ect of the DC electric fi eld / current on the crack healing behavior was examined in 8mol % yttria – stabilized cubic zirconia ( 8Y – CSZ ) polycrystals. Microcracks formed in 8Y – CSZ using the micro Vickers technique was healed under the fl ash conditions at sample temperatures of 1040 ℃ and 1230 ℃ by controlling the DC electric fi eld / current. At high temperatures, releasing the external energies, which were stored by the indentation as the elastic / plastic strains and new crack surfaces, would be driving forces for the crack healing. Thus, the crack healing takes place some extent even for the static annealing without the DC electric fi eld / current and the healing length becomes larger in the cracks formed at the larger loads. As compared to the static annealing, the healing behavior was accelerated by several times under the fl ash event condition even at the same temperatures. This suggests that the accelerated healing behavior cannot be explained only by the thermal activated processes, but ascribed to non – thermal processes accelerated by the fl ash event. Since the grain growth behavior was accelerated under the fl ash condition, the fl ash event enhanced the healing behavior of the microcrack damages by accelerating the di ff usional processes.
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利用Flash事件修复立方氧化锆(8Y-CSZ)微裂纹
研究了直流电场/电流对8mol %氧化钇稳定立方氧化锆(8Y - CSZ)多晶裂纹愈合行为的影响。通过控制直流电场/电流,在1040℃和1230℃的灰化条件下,用显微维氏法在8Y - CSZ上形成的微裂纹被修复。在高温下,压痕中储存的外部能量以弹/塑性应变和新裂纹表面的形式释放,将成为裂纹愈合的驱动力。因此,即使在没有直流电场/电流的静态退火条件下,裂纹也会发生一定程度的愈合,并且在较大载荷下形成的裂纹中愈合长度变大。与静态退火相比,即使在相同温度下,灰事件条件下的愈合行为也加快了数倍。这表明,加速愈合行为不能仅仅用热激活过程来解释,而应归因于由火山灰事件加速的非热过程。粉煤灰加速了微裂纹损伤的生长行为,从而加速了微裂纹损伤的扩散过程,增强了微裂纹损伤的愈合行为。
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