Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing

Q2 Chemistry Current Chemistry Letters Pub Date : 2022-01-01 DOI:10.5267/j.ccl.2021.9.002
K. Hassan, Elkhabiry Shaban, G. Elhaddad, Asmaa B. Sallam, I. Sayed
{"title":"Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing","authors":"K. Hassan, Elkhabiry Shaban, G. Elhaddad, Asmaa B. Sallam, I. Sayed","doi":"10.5267/j.ccl.2021.9.002","DOIUrl":null,"url":null,"abstract":"A series of azo dyes incorporated acridine chromophore labelled as 8 (a-d), 10 (a, b), 12 and 14 were prepared in very good yields starting from 9-chloroacridine 1 followed by amination, diazotization and coupling either with rhodanine analogues 6 (a, b) or other coupling partners 9 (a, b), 11 and 13. FT-IR, 1H NMR, and mass spectroscopic analysis were used to establish the structures of the produced azo dispersed dyes. Moreover, the synthesized azo dyes were used to prepare pastes that were used to print polyester fabric using classic silk-screen printing techniques. The dyes were tested for color strength and fastness properties, and they showed good fastness resistance to washing, rubbing, and perspiration, as well as fastness to sublimation and light. The dyes were further screened for their in vitro antibacterial activity against both Gram (+) and Gram (-) bacterial species. Most of them showed promising activities against these tested organisms.","PeriodicalId":10942,"journal":{"name":"Current Chemistry Letters","volume":"27 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Current Chemistry Letters","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5267/j.ccl.2021.9.002","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"Chemistry","Score":null,"Total":0}
引用次数: 2

Abstract

A series of azo dyes incorporated acridine chromophore labelled as 8 (a-d), 10 (a, b), 12 and 14 were prepared in very good yields starting from 9-chloroacridine 1 followed by amination, diazotization and coupling either with rhodanine analogues 6 (a, b) or other coupling partners 9 (a, b), 11 and 13. FT-IR, 1H NMR, and mass spectroscopic analysis were used to establish the structures of the produced azo dispersed dyes. Moreover, the synthesized azo dyes were used to prepare pastes that were used to print polyester fabric using classic silk-screen printing techniques. The dyes were tested for color strength and fastness properties, and they showed good fastness resistance to washing, rubbing, and perspiration, as well as fastness to sublimation and light. The dyes were further screened for their in vitro antibacterial activity against both Gram (+) and Gram (-) bacterial species. Most of them showed promising activities against these tested organisms.
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
偶氮杂化吖啶发色团的合成、表征、抗菌活性及其在聚酯印花中的应用
从9-氯吖啶1开始,通过胺化、重氮化和与罗丹宁类似物6 (A, b)或其他偶联伙伴9 (A, b)、11和13偶氮化,以很好的收率制备了一系列含有吖啶发色团的偶氮染料,标记为8 (A -d)、10 (A, b)、12和14。利用红外光谱(FT-IR)、核磁共振氢谱(1H NMR)和质谱分析确定了偶氮分散染料的结构。此外,合成的偶氮染料被用来制备浆料,用于用经典的丝网印刷技术印刷聚酯织物。对染料的色强和牢度性能进行了测试,结果表明,染料具有良好的耐洗涤、耐摩擦、耐汗水、耐升华和耐光照的牢度。进一步筛选染料对革兰氏(+)和革兰氏(-)细菌的体外抗菌活性。其中大多数对这些被试生物显示出有希望的活性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
Current Chemistry Letters
Current Chemistry Letters Chemistry-Chemistry (all)
CiteScore
4.90
自引率
0.00%
发文量
27
审稿时长
20 weeks
期刊介绍: The "Current Chemistry Letters" is a peer-reviewed international journal which aims to publish all the current and outstanding research articles, reviews and letters in chemistry including analytical chemistry, green chemistry, inorganic chemistry, organic chemistry, physical chemistry, etc. This journal is dedicated to serve all academic and industrial researchers and scientists who are expert in all major advances in chemistry research. The journal aims to provide the most complete and reliable source of information on current developments in these fields. The emphasis will be on publishing quality articles rapidly and openly available to researchers worldwide. Please note readers are free to read, download, copy, distribute, print, search, or link to the full texts of articles published on this journal. Current Chemistry Letters is an open access journal, which provides instant access to the full text of research papers without any need for a subscription to the journal where the papers are published. Therefore, anyone has the opportunity to copy, use, redistribute, transmit/display the work publicly and to distribute derivative works, in any sort of digital form for any responsible purpose, subject to appropriate attribution of authorship. Authors who publish their articles may also maintain the copyright of their articles.
期刊最新文献
Thermal and morphological studies of chitosan and agar-agar blends In vitro biological assessment of 1,3,4-oxadiazole sandwiched by azinane and acetamides supported by molecular docking and BSA binding studies Effect of different concentrations and combinations of some plant growth regulators on Punica granatum anther culture Design, synthesis and characterization of some new pyrazol-pyrimidine derivatives and evaluation of their biological activities Quantification of Alectinib in spiked rabbit plasma using liquid chromatography- electro spray ionization-tandem mass spectrophotometry: An application to pharmacokinetic study
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1