K. Hansongnern, Uraiwan Changsaluk, C. Pakawatchai
{"title":"Crystal Structure of 5-Methyl-2-(phenylazo)pyridine","authors":"K. Hansongnern, Uraiwan Changsaluk, C. Pakawatchai","doi":"10.2116/ANALSCIX.24.X99","DOIUrl":null,"url":null,"abstract":"The title compound, C12H11N3, was synthesized and characterized by X-ray diffraction analysis. In the molecule, the substituted pyridine ring is not coplanar with the azo group, and the angle between the pyridine ring and the azo plane is 7.6(2)°. However, the angle between the azo plane and the benzene ring is 9.7(2)°. The N=N distance is 1.228(2)A.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"26 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Sciences: X-ray Structure Analysis Online","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2116/ANALSCIX.24.X99","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
Abstract
The title compound, C12H11N3, was synthesized and characterized by X-ray diffraction analysis. In the molecule, the substituted pyridine ring is not coplanar with the azo group, and the angle between the pyridine ring and the azo plane is 7.6(2)°. However, the angle between the azo plane and the benzene ring is 9.7(2)°. The N=N distance is 1.228(2)A.
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