Electro-Polymerized Titan Yellow Modified Carbon Paste Electrode for the Analysis of Curcumin

Surfaces Pub Date : 2021-07-23 DOI:10.3390/SURFACES4030017
Edwin S. D’Souza, J. G. Manjunatha, C. Raril, Girish Tigari, H. J. Arpitha, Suvarnalatha Shenoy
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引用次数: 3

Abstract

A modest, efficient, and sensitive chemically modified electrode was fabricated for sensing curcumin (CRC) through an electrochemically polymerized titan yellow (TY) modified carbon paste electrode (PTYMCPE) in phosphate buffer solution (pH 7.0). Cyclic voltammetry (CV) linear sweep voltammetry (LSV) and differential pulse voltammetry (DPV) approaches were used for CRC detection. PTYMCPE interaction with CRC suggests that the electrode exhibits admirable electrochemical response as compared to bare carbon paste electrode (BCPE). Under the optimized circumstances, a linear response of the electrode was observed for CRC in the concentration range 2 × 10−6 M to 10 × 10−6 M with a limit of detection (LOD) of 10.94 × 10−7 M. Moreover, the effort explains that the PTYMCPE electrode has a hopeful approach for the electrochemical resolution of biologically significant compounds. Additionally, the proposed electrode has demonstrated many advantages such as easy preparation, elevated sensitivity, stability, and enhanced catalytic activity, and can be successfully applied in real sample analysis.
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电聚合泰坦黄修饰碳糊电极分析姜黄素
采用磷酸缓冲液(pH 7.0)中电化学聚合的土豆黄(TY)修饰碳糊电极(PTYMCPE)制备了一种小巧、高效、灵敏的姜黄素(CRC)传感电极。采用循环伏安法(CV)、线性扫描伏安法(LSV)和差分脉冲伏安法(DPV)检测结直肠癌。PTYMCPE与CRC的相互作用表明,与裸碳糊电极(BCPE)相比,PTYMCPE具有良好的电化学响应。在优化条件下,在2 × 10−6 M ~ 10 × 10−6 M的浓度范围内,电极对CRC具有良好的线性响应,检出限为10.94 × 10−7 M。此外,该研究表明PTYMCPE电极为生物重要化合物的电化学解析提供了一种有希望的方法。此外,该电极具有制备简单、灵敏度高、稳定性好、催化活性强等优点,可成功应用于实际样品分析。
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