Effect of Using Different Preparation Methods on the Properties of CdS Nanoparticles

Nada K. Abbas, Zainab Yaaqoub
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引用次数: 1

Abstract

This study aims to prepare cadmium sulfide nanoparticles in two methods, which are the chemical method and the biological method using two types of extracts, green tea, and starch. The prepared nanoparticles were characterized by various techniques such as X-ray diffraction (XRD), scanning electron microscope (SEM), and Energy Dispersive X-ray Spectroscopy (EDX). The synthesis of crystalline CdS nanoparticles was confirmed by various analytical techniques such as X-ray diffraction (XRD) and the pattern reveals cubic and hexagonal structures. The average crystal size for the methods respectively is 11.5, 15.9, and 5.67 nm, which have a spherical shape for nanoparticles CdS by scanning electron microscopy (SEM). The peaks of cadmium and sulfur emerged in the assay (EDX). The energy gap of the CdS has increased than the energy gap of the bulk CdS, the results were 2.63, 2.88, and 3.06 eV, respectively. This is an evidence of obtaining a nano-material for CDS by these two methods.
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不同制备方法对CdS纳米颗粒性能的影响
本研究以绿茶和淀粉两种提取物为原料,采用化学方法和生物方法制备硫化镉纳米颗粒。利用x射线衍射(XRD)、扫描电子显微镜(SEM)和能量色散x射线能谱(EDX)等技术对制备的纳米颗粒进行了表征。通过x射线衍射(XRD)等多种分析技术证实了CdS纳米颗粒的合成,其图案显示出立方和六边形结构。扫描电镜显示,这三种方法制备的纳米CdS的平均晶粒尺寸分别为11.5 nm、15.9 nm和5.67 nm,具有球形结构。在EDX分析中出现镉和硫的峰。CdS的能隙比块体CdS的能隙增大,分别为2.63、2.88和3.06 eV。这是通过这两种方法获得CDS纳米材料的一个证据。
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