Synthesis of cobalt aluminates by using the peel extracts of Citrus family species

IF 1.3 4区 化学 Q3 CHEMISTRY, MULTIDISCIPLINARY Main Group Chemistry Pub Date : 2023-01-20 DOI:10.3233/mgc-220099
F. T. S. Dumanli, Enis Muhammet Gul, E. Derun
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Abstract

Synthesis of cobalt aluminate was achieved by using the peel extracts of Citrus family species. The peel extracts of lemon, orange and mandarin were used as capping agent in experimental step. These peels were extracted through varied solvents including water, ethanol and methanol. In this regard, the efficacies of the peel type and the extraction liquid were surveyed in the study, using a co-precipitation technique in the synthesis of CoAl2O4 spinel. Samples compared in different parameters were subjected to a range of analyses consisting of colorimetry, X-Ray Diffraction, Scanning Electron Microscope and thermal examinations. The minimum b * value was reached as –14.23 in the sample with a capping agent provided by the orange peel extract, extraction liquid of which is water. The results denoted successful crystal structure scores and single-phase CoAl2O4 formation as well as the occurrence of a double-phase configuration. The highest XRD score of 83 was obtained for CoAl2O4. Considering SEM results, the lowest and highest particle size distributions were found between 100–150 nm and 350–800 nm, respectively. In the research, cobalt aluminate synthesis was carried out by means of modifying agents prepared with the peels of Citrus family species using different solvents.
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利用柑橘科植物果皮提取物合成铝酸钴
以柑橘科植物的果皮提取物为原料合成了铝酸钴。在实验步骤中,以柠檬、橘子和柑桔皮提取物为封盖剂。这些果皮通过不同的溶剂提取,包括水、乙醇和甲醇。为此,采用共沉淀法,考察了剥离类型和萃取液在合成CoAl2O4尖晶石中的效果。在不同参数下比较的样品进行了一系列分析,包括比色法、x射线衍射、扫描电子显微镜和热检查。用橙皮提取物提供的盖层剂,提取液为水,样品的b *值最小为-14.23。结果表明,晶体结构得分成功,形成了单相的CoAl2O4,并出现了双相结构。其中,CoAl2O4的XRD得分最高,为83分。SEM结果显示,在100 ~ 150 nm和350 ~ 800 nm之间,粒径分布最小,粒径分布最大。本研究以柑橘科植物的果皮为原料,采用不同溶剂制备改性剂,合成了铝酸钴。
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来源期刊
Main Group Chemistry
Main Group Chemistry 化学-化学综合
CiteScore
2.00
自引率
26.70%
发文量
65
审稿时长
>12 weeks
期刊介绍: Main Group Chemistry is intended to be a primary resource for all chemistry, engineering, biological, and materials researchers in both academia and in industry with an interest in the elements from the groups 1, 2, 12–18, lanthanides and actinides. The journal is committed to maintaining a high standard for its publications. This will be ensured by a rigorous peer-review process with most articles being reviewed by at least one editorial board member. Additionally, all manuscripts will be proofread and corrected by a dedicated copy editor located at the University of Kentucky.
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