Structural and Morphological Characterization of MEH-PPV Nanocomposite Doped with FeCl3

Noor M. Jabbar, Mustafa M- A. Hussein
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Abstract

Poly [2-methoxy-5-(2-ethylhexyloxy)-1, 4-phenylenevinyl] (MEH-PPV) thin films were created in this study using both spin coating and drop casting processes. MEH-PPV thin films generated by Ferric Chloride (FeCl3) doping (0.03, 0.06, 0.09, and 0.12 wt%) were studied for some physical features using Fourier-Transform Infrared Spectroscopy (FTIR), Field Emission Scanning Electron Microscopy (FE-SEM), and Energy Dispersive X-ray Spectroscopy (EDX). An FTIR test showed that there was no chemical reaction that occurred between Ferric Chloride (FeCl3) and MEH-PPV, but rather a physical one, that is, an organic material composite occurred. As for FE-SEM, the pure sample MEH-PPV formed uniformly, but when FeCl3 was added by weight, we have different circles that indicate the formation of adsorption energy and that the highest adsorption energy appears at MEH-PPV/FeCl3 (0.06%), as well as EDX, which indicates the absence of undesirable elements and indicates the presence of small peaks for iron (Fe) and chlorine (Cl). Peaks of carbon(C) and oxygen (O) types indicate the presence of the chemical elements of MEH-PPV.
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掺杂FeCl3的MEH-PPV纳米复合材料的结构与形态表征
采用自旋镀膜和滴铸法制备了聚[2-甲氧基-5-(2-乙基己氧基)- 1,4 -苯基乙烯基](MEH-PPV)薄膜。采用傅里叶变换红外光谱(FTIR)、场发射扫描电镜(FE-SEM)和能量色散x射线光谱(EDX)研究了氯化铁(FeCl3)掺杂(0.03、0.06、0.09和0.12 wt%)制备的MEH-PPV薄膜的一些物理特征。FTIR测试表明,氯化铁(FeCl3)与MEH-PPV之间没有发生化学反应,而是发生了物理反应,即有机材料复合。在Fe - sem上,纯样品MEH-PPV形成均匀,但当重量添加FeCl3时,我们有不同的圆圈表示吸附能的形成,最高的吸附能出现在MEH-PPV/FeCl3(0.06%)处,以及EDX处,这表明不存在不良元素,并且铁(Fe)和氯(Cl)存在小峰。碳(C)型和氧(O)型峰表明存在MEH-PPV的化学元素。
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