Study of the Structural and Mechanical Properties of Recycled High Density Polyethylene/Palm Kernel Shell Ash Bio-Composite

C. Agbo, B. A. Okorie, H. K. Idu
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Abstract

This study examined the structure and mechanical properties of recycled high density polyethylene(RHDPE)/palm kernel shell ash (PKSA) bio-composite. The reinforcement was added to the polymer matrix in concentrations of 5, 10, 15, 20 and 25wt% and particle sizes of 100, 150, 200, 250, 300µm. The composite samples were produced using injection moulding technique and subjected to mechanical and tribological property tests for percentage elongation, ultimate tensile strength, and hardness. The structure of the composite samples was analyzed using an optical metallurgical microscope. Results of the structural analysis revealed that the reinforcement of small particle size (100µm) formed a better interfacial bond with the polymer matrix compared with that of other particles sizes. The structural analysis also revealed uniform distribution of hard and brittle particles of the reinforcement in the polymer matrix. Mechanical test results showed that addition of palm kernel shell ash to the polymer matrix decreased its percentage elongation and impact strength by 24.5% and 22% respectively but significantly increased the tensile strength and hardness by 107.9% and 72% respectively. The ultimate tensile strength, and hardness of the developed composite increased with decrease in reinforcement particle size. Maximum ultimate tensile strength of 131MPa was obtained by the RHDP containing 10wt% PKSA of 100µm particle size while maximum hardness value of 86BHN was obtained at 25wt% palm kernel shell ash of 100µm particle size addition. Palm kernel shell ash reinforced recycled high density polyethylene bio-composite of improved mechanical properties that can be applied in production of engineering components. Keywords: Palm kernel shell ash, RHDPE, Percentage elongation, Ultimate tensile strength, Hardness. DOI : 10.7176/CPER/62-05 Publication date: January 31 st 2020
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再生高密度聚乙烯/棕榈仁壳灰生物复合材料的结构与力学性能研究
研究了再生高密度聚乙烯(RHDPE)/棕榈仁壳灰(PKSA)生物复合材料的结构和力学性能。在聚合物基体中添加浓度分别为5%、10%、15%、20%和25wt%,粒径分别为100、150、200、250、300µm的增强剂。复合材料样品采用注射成型技术生产,并进行了机械和摩擦学性能测试,包括伸长率、极限拉伸强度和硬度。利用光学金相显微镜对复合材料的组织进行了分析。结构分析结果表明,与其他粒径的增强剂相比,小粒径(100µm)的增强剂与聚合物基体形成了更好的界面结合。结构分析还揭示了增强材料在聚合物基体中的硬脆颗粒均匀分布。力学试验结果表明,棕榈仁壳灰的加入使聚合物基体的伸长率和冲击强度分别降低了24.5%和22%,而拉伸强度和硬度分别显著提高了107.9%和72%。复合材料的极限抗拉强度和硬度随增强颗粒尺寸的减小而增大。当PKSA含量为10wt%,粒径为100µm时,RHDP的最大抗拉强度为131MPa;当棕榈仁壳灰含量为25wt%,粒径为100µm时,RHDP的最大硬度为86BHN。棕榈仁壳灰增强再生高密度聚乙烯生物复合材料的力学性能得到改善,可应用于工程部件的生产。关键词:棕榈仁灰,RHDPE,伸长率,极限抗拉强度,硬度。DOI: 10.7176/CPER/62-05出版日期:1月31日2020
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