Preparation and Characterization of Treated MWCNT-Muscovite Filled Epoxy Nanocomposites

Procedia Chemistry Pub Date : 2016-01-01 DOI:10.1016/j.proche.2016.03.009

Nur Suraya Anis Ahmad Bakhtiar , Yeap Cheok Kuang , Siti Shuhadah Md. Saleh , Hazizan Md Akil

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引用次数: 3

Abstract

This paper presents the surface treatment of multiwalled carbon nanotube (MWCNT)/muscovite (MUS) hybrid nanomaterial. The hybrid compound was synthesized by chemical vapor deposition (CVD) using methane as the carbon precursor. Morphological characterization of treatment and pristine MWCNT-MUS hybrid was conducted using Field Emission Scanning Electron Microscope (FESEM) and X–ray diffraction (XRD). The surface treatment of MWCNT/MUS hybrid nanomaterial was successfully carried out which the basal spacing of (001) plane d₍₀₀₁₎ of MCNT/MUS was enlarged from 21.00 Å to 27.20 Å after first stage after first stage and was further enlarged to 29.28 Å after second stage of CTAB treatment. This MCNT-MUS hybrid filler was incorporated into epoxy resin at different filler loadings (0.5, 1.0, and 1.5 wt %). Thermal properties of the treated Epoxy/MWCNT-MUS was determined to have lower properties compared to pristine Epoxy/MWCNT-MUS.

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mwcnt -白云母填充环氧纳米复合材料的制备与表征

介绍了多壁碳纳米管/白云母杂化纳米材料的表面处理方法。以甲烷为碳前驱体，采用化学气相沉积(CVD)法制备了该杂化化合物。利用场发射扫描电镜(FESEM)和x射线衍射(XRD)对处理后的MWCNT-MUS和原始MWCNT-MUS杂交体进行了形态表征。成功地进行了MWCNT/MUS杂化纳米材料的表面处理，经过一段又一段的处理，MCNT/MUS的(001)面d(001)基间距从21.00 Å扩大到27.20 Å，经过第二段的CTAB处理，进一步扩大到29.28 Å。该MCNT-MUS混合填料以不同的填料负荷(0.5、1.0和1.5 wt %)掺入环氧树脂中。经处理的环氧树脂/MWCNT-MUS的热性能与原始环氧树脂/MWCNT-MUS相比，具有较低的性能。

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Procedia Chemistry

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