Electron beam additive manufacturing of TiB2/Ti–6Al–4V composite

A. Panin, M. Kazachenok, L. Kazantseva, S. Martynov, M. Korchagin
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Abstract

Microstructure and phase composition of the titanium matrix composite made from a pre-mixed powder blend of Ti–6Al–4V+TiB2 were studied. High energy planetary ball milling method was used both to obtain TiB2 powder and to mix Ti–6Al–4V matrix composite powder with 5 wt.% TiB2. Electron beam melting technology was used to build the parts of the titanium metal matrix composites. To modify the microstructure of additive manufactured TiB2/Ti–6Al–4V sample their surface layer was subjected to one-pass electron beam melting. It was shown that the microstructure of 3D- printed TiB2/Ti–6Al–4V sample consists of equiaxial prior β grains of approximately 200 µm in size with the acicular α phase. TiB phase formation in the as-build titanium matrix composite was found. Subsequent electron beam surface treatment decreased in the width of acicular α phase and increased in the volume fraction of β phase in the titanium matrix composite.Microstructure and phase composition of the titanium matrix composite made from a pre-mixed powder blend of Ti–6Al–4V+TiB2 were studied. High energy planetary ball milling method was used both to obtain TiB2 powder and to mix Ti–6Al–4V matrix composite powder with 5 wt.% TiB2. Electron beam melting technology was used to build the parts of the titanium metal matrix composites. To modify the microstructure of additive manufactured TiB2/Ti–6Al–4V sample their surface layer was subjected to one-pass electron beam melting. It was shown that the microstructure of 3D- printed TiB2/Ti–6Al–4V sample consists of equiaxial prior β grains of approximately 200 µm in size with the acicular α phase. TiB phase formation in the as-build titanium matrix composite was found. Subsequent electron beam surface treatment decreased in the width of acicular α phase and increased in the volume fraction of β phase in the titanium matrix composite.
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TiB2/ Ti-6Al-4V复合材料的电子束增材制造
研究了Ti-6Al-4V +TiB2预混合粉末共混制备的钛基复合材料的显微组织和相组成。采用高能行星球磨法制备TiB2粉末,并与5wt .% TiB2混合制备Ti-6Al-4V基复合粉末。采用电子束熔化技术制备钛金属基复合材料的零件。为了改善添加剂制备的TiB2/ Ti-6Al-4V样品的微观结构,对其表层进行了一次电子束熔化处理。结果表明,3D打印TiB2/ Ti-6Al-4V样品的微观结构由大小约为200µm的等轴先验β晶粒和针状α相组成。发现钛基复合材料中存在TiB相。随后的电子束表面处理减小了钛基复合材料中针状α相的宽度,增大了β相的体积分数。研究了Ti-6Al-4V +TiB2预混合粉末共混制备的钛基复合材料的显微组织和相组成。采用高能行星球磨法制备TiB2粉末,并与5wt .% TiB2混合制备Ti-6Al-4V基复合粉末。采用电子束熔化技术制备钛金属基复合材料的零件。为了改善添加剂制备的TiB2/ Ti-6Al-4V样品的微观结构,对其表层进行了一次电子束熔化处理。结果表明,3D打印TiB2/ Ti-6Al-4V样品的微观结构由大小约为200µm的等轴先验β晶粒和针状α相组成。发现钛基复合材料中存在TiB相。随后的电子束表面处理减小了钛基复合材料中针状α相的宽度,增大了β相的体积分数。
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