Liang Huang, Pinxian Xi, Min Xu, Tonghuan Liu, Z. Zeng
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引用次数: 3
Abstract
The title compound, C14H24N6O4S, was prepared by the reaction of ethyl N-(3-tossulfonyl)carbamate with metformin. It was crystallized in the triclinic system, space group P1 with a = 6.894(3)A, b = 8.323(4)A, c = 17.184(8)A, α = 84.119(7)°, β = 84.028(6)°, γ = 75.479(6)°, V = 946.4(7)A3, Z = 2, R = 0.0426. The molecules are linked by two kinds of hydrogen-bonds, N-H…N and N-H…O, generating an extended two-dimensional supramolecular network structure in the ab plane.
以甲双胍为原料，N-(3-磺酰基)氨基甲酸乙酯为原料，合成了标题化合物C14H24N6O4S。在三斜晶系P1中，空间群a = 6.894(3) a, b = 8.323(4) a, c = 17.184(8) a， α = 84.119(7)°，β = 84.028(6)°，γ = 75.479(6)°，V = 946.4(7)A3, Z = 2, R = 0.0426。分子由两种氢键N- h…N和N- h…O连接，在ab平面上形成扩展的二维超分子网络结构。
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