Microwave-assisted Synthesis of Zinc Oxide Nanoparticles

M. Hasanpoor, M. Aliofkhazraei, H. Delavari
{"title":"Microwave-assisted Synthesis of Zinc Oxide Nanoparticles","authors":"M. Hasanpoor,&nbsp;M. Aliofkhazraei,&nbsp;H. Delavari","doi":"10.1016/j.mspro.2015.11.101","DOIUrl":null,"url":null,"abstract":"<div><p>Synthesis of nanoparticles and ultrafine particles of zinc oxide with controlled morphology using microwave irradiation is carried out by various methods. The effect of type of precursor as well as the time and the microwave irradiation power on the structure and size of ZnO nanoparticles have been studied. Particles Studied by SEM, TEM images and XRD analyze. By increasing the time of synthesis from 10 to 15<!--> <!-->minutes needle-shaped particles with a diameter of 50-150<!--> <!-->nm can be achieved. While increasing the microwave power from 540 to 680 watts, flower-shaped particles are obtained. By replacing zinc nitrate with zinc acetate, at different power and time of irradiation, needle-shaped particles are obtained and diameter of needles is decreased.</p></div>","PeriodicalId":101041,"journal":{"name":"Procedia Materials Science","volume":"11 ","pages":"Pages 320-325"},"PeriodicalIF":0.0000,"publicationDate":"2015-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/j.mspro.2015.11.101","citationCount":"151","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Procedia Materials Science","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2211812815004435","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 151

Abstract

Synthesis of nanoparticles and ultrafine particles of zinc oxide with controlled morphology using microwave irradiation is carried out by various methods. The effect of type of precursor as well as the time and the microwave irradiation power on the structure and size of ZnO nanoparticles have been studied. Particles Studied by SEM, TEM images and XRD analyze. By increasing the time of synthesis from 10 to 15 minutes needle-shaped particles with a diameter of 50-150 nm can be achieved. While increasing the microwave power from 540 to 680 watts, flower-shaped particles are obtained. By replacing zinc nitrate with zinc acetate, at different power and time of irradiation, needle-shaped particles are obtained and diameter of needles is decreased.

查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
微波辅助合成氧化锌纳米颗粒
采用多种方法在微波照射下合成形貌可控的氧化锌纳米颗粒和超细颗粒。研究了前驱体类型、微波辐照时间和微波辐照功率对ZnO纳米颗粒结构和尺寸的影响。对颗粒进行了SEM、TEM和XRD分析。将合成时间从10分钟增加到15分钟,可以得到直径为50 ~ 150nm的针状颗粒。当微波功率从540瓦增加到680瓦时,可以得到花状粒子。用乙酸锌代替硝酸锌,在不同辐照功率和辐照时间下,得到针状颗粒,针状颗粒直径减小。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
On Fatigue Behaviour of Two Spring Steels. Part II: Mathematical Models Analysis and Modeling of Depolarization Effects in Mueller Matrix Spectroscopic Ellipsometry Data Proximity Factor on Transformation from Subsurface to Surface Flaw Determination of Anisotropic Crystal Optical Properties Using Mueller Matrix Spectroscopic Ellipsometry Diffusion of Hydrogen in the TRIP 800 Steel
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1