{"title":"Nouvelle cuve chauffante et evacuable pour l'infra-rouge","authors":"V. Tabacik","doi":"10.1016/0371-1951(66)80150-9","DOIUrl":null,"url":null,"abstract":"<div><p>The details of the construction of a cell for the measurement, in the gase phase, of IR absorption spectra of crystalline substances is described. The cell can be evacuated to 10<sup>−5</sup> mm Hg, heated to 250°C, and is equipped with interchangeable windows; its volume is approximately 100 ml and the optical path is 10 cm. The measurable quantity of substance is on the order of a few tens of milligrams and the substance is quantitatively recovered in a pure state after the measurement. Some problems posed by the functioning and the maintenance of the cell, as well as the advantages of the method, are discussed.</p></div>","PeriodicalId":101180,"journal":{"name":"Spectrochimica Acta","volume":"22 8","pages":"Pages 1530-1532"},"PeriodicalIF":0.0000,"publicationDate":"1966-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0371-1951(66)80150-9","citationCount":"3","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Spectrochimica Acta","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/0371195166801509","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3
Abstract
The details of the construction of a cell for the measurement, in the gase phase, of IR absorption spectra of crystalline substances is described. The cell can be evacuated to 10−5 mm Hg, heated to 250°C, and is equipped with interchangeable windows; its volume is approximately 100 ml and the optical path is 10 cm. The measurable quantity of substance is on the order of a few tens of milligrams and the substance is quantitatively recovered in a pure state after the measurement. Some problems posed by the functioning and the maintenance of the cell, as well as the advantages of the method, are discussed.