Nouvelle cuve chauffante et evacuable pour l'infra-rouge

V. Tabacik
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引用次数: 3

Abstract

The details of the construction of a cell for the measurement, in the gase phase, of IR absorption spectra of crystalline substances is described. The cell can be evacuated to 10−5 mm Hg, heated to 250°C, and is equipped with interchangeable windows; its volume is approximately 100 ml and the optical path is 10 cm. The measurable quantity of substance is on the order of a few tens of milligrams and the substance is quantitatively recovered in a pure state after the measurement. Some problems posed by the functioning and the maintenance of the cell, as well as the advantages of the method, are discussed.

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新的加热和可疏散的红外线容器
在气相中,描述了用于测量晶体物质红外吸收光谱的细胞的结构细节。该电池可以被疏散到10−5毫米汞柱,加热到250°C,并配备可互换的窗口;其体积约为100毫升,光程为10厘米。该物质的可测量量在几十毫克量级,测量后该物质在纯净状态下被定量回收。讨论了细胞的功能和维护所带来的一些问题,以及该方法的优点。
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