Effect of different concentrations of propylene glycol on the physical-chemical properties of MTA

IF 0.5 Q4 DENTISTRY, ORAL SURGERY & MEDICINE Giornale Italiano di Endodonzia Pub Date : 2021-04-07 DOI:10.32067/GIE.2021.35.01.10
Daniela Peressoni Vieira Schuldt, L. F. R. Garcia, C. Teixeira, Beatriz Dulcineia Mendes Souza, Julia Menezes Savaris, E. A. Bortoluzzi
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引用次数: 1

Abstract

Aim: This study evaluated the effect of different concentrations of propylene glycol (PG) on the dimensional change (DC), compressive strength (CS), solubility and pH of MTA. Methodology: Groups were formed according to the proportion of distilled water (DW) and PG in MTA manipulation: G1 (100% DW); G2 (80% DW+20% PG); G3 (50% DW+50% PG); G4 (20% DW+80% PG). The tests were guided by ISO and BSI standards. DC and CS tests were performed after 24 h and 30 days of samples storage in water. In the solubility test, rings filled with the cements were weighed after setting and after 7 days. The pH was measured after 3 and 24 h, and 30 days. The data were analyzed with the ANOVA, Tukey’s and Paired t tests (a=5%). Results: After 24 h and 30 days, the DC and CS were similar among groups, except the CS for G3 in 30 days. After 7 days, G1 gained weight when hydrated, differing from G3 and G4 (p<0.05). When weighed dehydrated, G2 was different from the other groups (p<0.05). After 3 h, G1 had lower pH values in comparison with G2, G3 and G4 (p<0.05). At the 24-h period, G2 had higher pH values than G1 and G2 (p<0.05). After 7 days, there was no difference among groups. Conclusions: PG did not affect the MTA dimensional change and compressive strength (except for G3). However, PG reduced MTA solubility (G2) and increased its pH after 3 hours.
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不同浓度丙二醇对MTA理化性质的影响
目的:研究不同浓度丙二醇(PG)对MTA的尺寸变化(DC)、抗压强度(CS)、溶解度和pH的影响。方法:按MTA操作中蒸馏水(DW)与PG的比例分组:G1组(100% DW);G2 (80% dw +20% pg);G3 (50% dw +50% pg);G4 (20% dw +80% pg)。测试以ISO和BSI标准为指导。样品在水中保存24 h和30 d后分别进行DC和CS试验。在溶解度测试中,分别在固井后和7天后对填充了胶结物的环进行称重。分别于3 h、24 h和30 d后测定pH。数据采用方差分析、Tukey’s检验和配对t检验(a=5%)进行分析。结果:在24 h和30 d时,除G3组在30 d时的CS外,各组间DC和CS基本相同。7 d后,G1在补水时体重增加,与G3和G4差异显著(p<0.05)。脱水称量后,G2与其他各组差异有统计学意义(p<0.05)。3 h后,G1的pH值低于G2、G3和G4 (p<0.05)。24 h时,G2的pH值高于G1和G2 (p<0.05)。7 d后,各组间无差异。结论:PG对MTA尺寸变化及抗压强度无明显影响(G3除外)。然而,PG降低了MTA的溶解度(G2),并在3小时后增加了其pH。
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来源期刊
Giornale Italiano di Endodonzia
Giornale Italiano di Endodonzia DENTISTRY, ORAL SURGERY & MEDICINE-
CiteScore
0.90
自引率
25.00%
发文量
0
审稿时长
24 weeks
期刊介绍: The Giornale Italiano di Endodonzia was founded in 1987 and is the official journal of the Italian Society of Endodontics (SIE). It is a peer-reviewed journal publishing original articles on clinical research and/or clinical methodology, case reports related to Endodontics. The Journal evaluates also contributes in restorative dentistry, dental traumatology, experimental pathophysiology, pharmacology and microbiology dealing with Endodontics.
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