Crystal Structure of Bis(4-methoxybenzoylmethylenetriparatolyl-phosphonium μ-Iodo(diiodomercurate)) Complex, C30H30HgI3O2P

S. Sabounchei, V. Jodaian, A. Dadrass, Hassan Nemattalab, H. Khavasi
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Abstract

The crystal structure of a colorless complex of [CH3OC6H4COCH2P(p·tolyl)3]2[Hg2I6] was determined by the X-ray diffraction method. All atoms occupy general positions in the monoclinic space group, P21/n and have the following unit-cell dimensions: a = 11.5933(11)A, b = 22.842(3)A, c = 12.2271(12)A, β = 103.719(8)°, Z = 4 and V = 3145.5(6)A3. The final R value is 0.0582.
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双(4-甲氧基苯甲酰亚甲基三对苯二酚-磷μ-碘(二碘氨基磺酸))配合物C30H30HgI3O2P的晶体结构
用x射线衍射法测定了无色配合物[CH3OC6H4COCH2P(p·托利基)3]2[Hg2I6]的晶体结构。所有原子在单斜空间群P21/n中占据一般位置,具有以下单位胞尺寸:a = 11.5933(11) a, b = 22.842(3) a, c = 12.2271(12) a, β = 103.719(8)°,Z = 4, V = 3145.5(6)A3。最终R值为0.0582。
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