S. Sabounchei, V. Jodaian, A. Dadrass, Hassan Nemattalab, H. Khavasi
{"title":"Crystal Structure of Bis(4-methoxybenzoylmethylenetriparatolyl-phosphonium μ-Iodo(diiodomercurate)) Complex, C30H30HgI3O2P","authors":"S. Sabounchei, V. Jodaian, A. Dadrass, Hassan Nemattalab, H. Khavasi","doi":"10.2116/ANALSCIX.24.X111","DOIUrl":null,"url":null,"abstract":"The crystal structure of a colorless complex of [CH3OC6H4COCH2P(p·tolyl)3]2[Hg2I6] was determined by the X-ray diffraction method. All atoms occupy general positions in the monoclinic space group, P21/n and have the following unit-cell dimensions: a = 11.5933(11)A, b = 22.842(3)A, c = 12.2271(12)A, β = 103.719(8)°, Z = 4 and V = 3145.5(6)A3. The final R value is 0.0582.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"16 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Sciences: X-ray Structure Analysis Online","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2116/ANALSCIX.24.X111","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
The crystal structure of a colorless complex of [CH3OC6H4COCH2P(p·tolyl)3]2[Hg2I6] was determined by the X-ray diffraction method. All atoms occupy general positions in the monoclinic space group, P21/n and have the following unit-cell dimensions: a = 11.5933(11)A, b = 22.842(3)A, c = 12.2271(12)A, β = 103.719(8)°, Z = 4 and V = 3145.5(6)A3. The final R value is 0.0582.
用x射线衍射法测定了无色配合物[CH3OC6H4COCH2P(p·托利基)3]2[Hg2I6]的晶体结构。所有原子在单斜空间群P21/n中占据一般位置,具有以下单位胞尺寸:a = 11.5933(11) a, b = 22.842(3) a, c = 12.2271(12) a, β = 103.719(8)°,Z = 4, V = 3145.5(6)A3。最终R值为0.0582。