O. Kapush, N. Mazur, A. Lysytsya, M. Moroz, B. Nechyporuk, B. Rudyk, V. Dzhagan, M. Valakh, V. Yukhymchuk
{"title":"Physical properties of nanocrystaline PbS synthesized by electrolytic method","authors":"O. Kapush, N. Mazur, A. Lysytsya, M. Moroz, B. Nechyporuk, B. Rudyk, V. Dzhagan, M. Valakh, V. Yukhymchuk","doi":"10.15330/pcss.24.2.262-268","DOIUrl":null,"url":null,"abstract":"The possibility of obtaining nanocrystaline lead sulfide by an electrolytic method using lead electrodes is demonstrated, and the influence of temperature on the synthesis process is investigated. Based on the results of X-ray diffraction studies, the chemical and phase composition of the obtained samples is determined, as well as the parameters of the unit cell of the crystals lattice. The size of the nanocrystallites and the magnitude of residual mechanical strain in them is determined using the methods of Debye-Scherrer and Williamson-Hall. The results of X-ray diffraction are in agreement with the results of the Raman scattering on phonons.","PeriodicalId":20137,"journal":{"name":"Physics and Chemistry of Solid State","volume":"118 1","pages":""},"PeriodicalIF":0.9000,"publicationDate":"2023-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Physics and Chemistry of Solid State","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.15330/pcss.24.2.262-268","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
Abstract
The possibility of obtaining nanocrystaline lead sulfide by an electrolytic method using lead electrodes is demonstrated, and the influence of temperature on the synthesis process is investigated. Based on the results of X-ray diffraction studies, the chemical and phase composition of the obtained samples is determined, as well as the parameters of the unit cell of the crystals lattice. The size of the nanocrystallites and the magnitude of residual mechanical strain in them is determined using the methods of Debye-Scherrer and Williamson-Hall. The results of X-ray diffraction are in agreement with the results of the Raman scattering on phonons.
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