Effect of Pretreatment Process on the Metal-Porcelain Bonding Mechanism and Properties of CoCr Alloy Dental Crown and Bridge Manufactured by SLM

IF 0.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY 稀有金属材料与工程 Pub Date : 2018-08-01 DOI:10.1016/S1875-5372(18)30187-5
Wang Di, Wu Shibiao, Fu Fan, Ye Guangzhao, Mai Shuzhen, Qian Zeyu, Song Changhui, Yang Yongqiang
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引用次数: 4

Abstract

This paper aims to investigate the influential mechanism of grinding and sand blasting pretreatment of CoCr alloy manufactured by SLM (selective laser melting) process on the metal-porcelain bonding of the restorations, and then provides references for SLM manufacturing CoCr alloy dental crown and bridge restorations with good mechanical properties. Three groups of CoCr alloy substrates were manufactured by SLM process with optimal parameters. The samples were subjected to different grinding and sand blasting pretreatment, and the porcelain sintering was carried out with the same parameters. The samples of different groups were analyzed by three-point bending test, roughness test, SEM and EDS. Results show that the metal-porcelain bonding strength of samples in group a with grinding and sand blasting is 36.79±0.49 MPa, which is obviously higher than those of group b with no grinding but sand blasting and group c with only grinding. The average metal-porcelain bonding strength of the three group samples is higher than the ISO9693: 1999 standard minimum 25 MPa. The metal-porcelain bonding effect of group a and c is better than that of group b, and the element diffusion on metal-porcelain interface is observed in all three groups. The results also show that there are significant differences among the three groups on residues and element distribution of metal-porcelain peeling surface. The final conclusion is that the surface roughness obtained by the pretreatment of sand blasting and grinding can ensure the strong chemical combination of metal and porcelain and considerable mechanical properties combination, which can improve the performance of metal-porcelain restorations manufactured by SLM.

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预处理工艺对SLM法制备CoCr合金牙冠和牙桥金属-瓷结合机理及性能的影响
本文旨在研究选择性激光熔化法制备的CoCr合金磨削和喷砂预处理对修复体金属-瓷结合的影响机理,为SLM法制备力学性能良好的CoCr合金牙冠和牙桥修复体提供参考。通过优化工艺参数,制备了三组CoCr合金基板。对样品进行不同的磨削和喷砂预处理,并在相同的参数下进行陶瓷烧结。采用三点弯曲试验、粗糙度试验、扫描电镜和能谱仪对不同组试样进行分析。结果表明:a组磨砂加喷砂试样的金属瓷结合强度为36.79±0.49 MPa,明显高于不磨砂加喷砂的b组和只磨砂的c组;三组样品的平均金属瓷结合强度均高于ISO9693: 1999标准最低25 MPa。a组和c组的金属-瓷结合效果好于b组,且三组金属-瓷界面上均存在元素扩散现象。结果还表明,三组金属瓷剥离表面的残留物和元素分布存在显著差异。最后得出结论:喷砂磨前处理获得的表面粗糙度可以保证金属与瓷的强化学结合和可观的力学性能组合,可以提高SLM制造的金属-瓷修复体的性能。
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来源期刊
稀有金属材料与工程
稀有金属材料与工程 工程技术-材料科学:综合
CiteScore
1.30
自引率
57.10%
发文量
17973
审稿时长
4.2 months
期刊介绍:
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