Comparative Study on The Structure, Physical Properties and Hardness Indentation of a Bulk Fill & An Incremental Composite Resin Restorative Materials

Amira Elsherbeny, R. Shalaby, Sayed M. Ghorab
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Abstract

Totally 80 disk-shaped specimens of Filtek™ Bulk-Fill, 3M ESPE, and Filtek™ Z250 XT, 3M ESPE, were prepared by using split-Teflon mold (4mm×10mm). Specimen characterization XRD, Surface roughness, degree of conversion, Surface microhardness, and depth of cure of the specimens were evaluated after the specimens were stored in distilled water in darkness at 37°C for 24 h. Statistical analysis was done using t-test with a significance level at p<0.05. FiltekTM Z350 XT showed the highest mean value of Vickers microhardness either on top surface 94.94% or bottom surface 69.92% and recorded 76.51% while FiltekTM Bulk-Fill was 66.85% for depth of cure. Filtek bulk-fill recorded a lower mean value of 0.73 for Surface roughness than FiltekTM Z350 XT and the highest degree of conversion of 84.34%. Statistical analysis showed that there was a significant difference between the mean values for all tested results. Increasing the filler content proved to have ability to enhance some properties, specially the surface roughness. Incorporation of some structurally rigid monomers like Bis-DMA, UDMA, TEGDMA within the resin matrix have a great influence on the measured properties, including degree of conversion reached to 84.34%, depth of cure to a level of 76.51% and Vickers microhardness to 94.94%.
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块状填料与增量复合树脂修复材料的结构、物理性能及硬度压痕比较研究
采用分离式teflon模具(4mm×10mm)制备了80个圆盘状的Filtek™Bulk-Fill, 3M ESPE和Filtek™Z250 XT, 3M ESPE样品。37℃蒸馏水黑暗保存24 h后,评价样品表征XRD、表面粗糙度、转化度、表面显微硬度、固化深度。采用t检验进行统计学分析,p<0.05为显著性水平。FiltekTM Z350 XT的维氏显微硬度平均值最高,上表面为94.94%,下表面为69.92%,为76.51%,而FiltekTM Bulk-Fill的固化深度为66.85%。Filtek填料的表面粗糙度平均值为0.73,低于FiltekTM Z350 XT,最高转化度为84.34%。统计分析表明,所有测试结果的平均值之间存在显著差异。事实证明,增加填料含量可以提高某些性能,特别是表面粗糙度。在树脂基体中掺入Bis-DMA、UDMA、TEGDMA等结构刚性单体对树脂的性能有较大影响,转化度达到84.34%,固化深度达到76.51%,维氏显微硬度达到94.94%。
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