Triglyceride Composition of Almond Seed Oil (Terminalia catappa) Grown in Nigeria using GC-MS and 1H-NMR Spectroscopy

Afolayan S. Sunday, Fashanu Titilope Abosede, Enenche E. Daniel, Adediji A. Yetunde, Salawu R. Adenike, Lawal Israel Oluwasanmi
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Abstract

Almond (Terminalia catappa) seeds are rich in oil; however, their study has received limited attention, with researches focused mainly on their health potentials. The present study assesses the composition of the fatty acid (FA) components present in the almond seed oils extracted using soxhlet apparatus and analysed by 1H-NMR (Proton Nuclear Magnetic Resonance) and Gas Chromatography Mass Spectrometry (GC-MS). Generally, there was significant agreement between the results from the 1H-NMR and GC-MS analyses, however, 1H NMR gave more reliable and reproducible results. The GC-MS and 1H NMR results revealed that the oils contained oleic acid (>18 %), linoleic (>28%) linolenic acid (≤0.03 %) and saturated fatty acids (>44 %).
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用GC-MS和1H-NMR分析尼日利亚产杏仁籽油的甘油三酯组成
杏仁(Terminalia catappa)种子富含油脂;然而,对它们的研究受到的关注有限,研究主要集中在它们的健康潜力上。本研究评估了用索氏装置提取的杏仁籽油中脂肪酸(FA)成分的组成,并通过1H-NMR(质子核磁共振)和气相色谱-质谱(GC-MS)进行了分析。一般来说,1H-NMR和GC-MS分析的结果有显著的一致性,然而,1H NMR给出了更可靠和可重复性的结果。GC-MS和1H NMR结果表明,油中含有油酸(> 18%)、亚油酸(>28%)、亚麻酸(≤0.03%)和饱和脂肪酸(> 44%)。
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