Hydroxyapatite formation of Ca and P modified micro-arc oxidation coating on Ti alloy

Liangwen Liu, Xin Wu, Jingyi Wang, N. Tang, Shuang Li, Xianjv Zhang, Mei Yang
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引用次数: 1

Abstract

ABSTRACT A Simulated Body Fluid (SBF) treatment was performed to modify the surface of a TiO2-based coating containing Ca and P prepared by micro-arc oxidation (MAO). Scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-Ray Photoelectron Spectroscopy (XPS) were employed to characterise the composition and morphology of the immersed Ca-P containing coating. The coating primarily presents a porous structure, which is mainly composed of anatase, rutile, CaP, and Nb2O5.The biological activity of the coating was determined by immersing in SBF for 5 days, showing hydroxyapatite (HA) formed on the surface of the coating and also revealing the good corrosion resistance of the coating in SBF. Finally, a lower MAO coating contact angle with SBF solution than that of TLM Ti alloy was obtained in the compatibility test, indicating that the coating has good compatibility with SBF.
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Ca和P改性钛合金微弧氧化涂层羟基磷灰石的形成
采用模拟体液(SBF)处理方法对微弧氧化法制备的含Ca和P的tio2基涂层进行表面修饰。采用扫描电子显微镜(SEM)、x射线衍射仪(XRD)和x射线光电子能谱仪(XPS)表征了浸没后的Ca-P涂层的组成和形貌。涂层主要呈多孔结构,主要由锐钛矿、金红石、CaP和Nb2O5组成。在SBF中浸泡5天,测定了涂层的生物活性,表明涂层表面形成了羟基磷灰石(HA),同时也表明涂层在SBF中具有良好的耐腐蚀性。
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