Estimation of distribution uniformity of Ti2NbAl particles in an aluminum-matrix composite material

I. E. Kalashnikov, L. Kobeleva, P. Bykov, A. Kolmakov, I. Katin, R. Mikheev
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Abstract

There was analyzed the distribution uniformity of reinforcing particles Ti2NbAl in composite materials (CM) based on aluminum alloy AO20-1, made by mechanical mixing. Samples with different structure dispersion were obtained by crystallization of a composite melt in molds made of materials with different thermal conductivity. There were used methods of digitizing the structure microphoto and mathematical statistics to estimation structural heterogeneity. Based on the results of processing the photographic images, there were constructed histograms of the frequencies of the distribution of intermetallic particles in the matrix. It is revealed that matrix structure refinement has positive effect on uniformity of the distribution. A significant decrease in the coefficient of variation for specimens with a finer structure also indicates a more uniform distribution of the reinforcing phase in this specimens. There was compared a wear resistance of the material and the uniformity of distribution of the Ti2NbAl powder in the matrix. A wear rate of composite materials was determined by testing on CETR UMT Multi-Specimen Test System under dry sliding friction conditions with sequential stepwise axial loading to values of 0.5, 1, 1.5, 2, 2.5, 3 MPa, at constant sliding speed of 0.5 m/s. The test time for each axial load was 2000 s, the friction path was 6000 m. It was observed a significant reduction in weight loss during friction for all CM samples as compared to the matrix alloy. The wear rate of CM specimens with a better distribution of the reinforcing component is reduced by more than 2.7 times as compared to specimens from the AO20-1 alloy, and with a less uniform distribution by 2.2 times
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铝基复合材料中Ti2NbAl颗粒分布均匀性的估计
分析了机械搅拌法制备的AO20-1铝合金复合材料(CM)中增强颗粒Ti2NbAl的分布均匀性。在不同导热系数材料的模具中对复合熔体进行结晶,得到了具有不同分散结构的样品。采用结构显微照片数字化和数理统计等方法对结构非均质性进行估计。根据图像处理结果,构建了金属间颗粒在基体中分布频率的直方图。结果表明,基体组织细化对组织均匀性有积极影响。结构越细的试样,其变异系数越小,表明其增强相分布越均匀。比较了材料的耐磨性和Ti2NbAl粉末在基体中的分布均匀性。在ctr UMT多试样试验系统上,以0.5 m/s的恒定滑动速度,轴向载荷依次为0.5、1、1.5、2、2.5、3 MPa,测试复合材料在干滑动摩擦条件下的磨损率。每个轴向载荷的试验时间为2000 s,摩擦路径为6000 m。与基体合金相比,观察到所有CM样品在摩擦期间的重量损失显著减少。增强成分分布较好的CM试样的磨损率比AO20-1合金试样降低了2.7倍以上,而增强成分分布不均匀的CM试样的磨损率降低了2.2倍
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