Preparation and Properties of Mg(OH)2 Whiskers by Ion Exchange Resin Method

Q2 Materials Science Revista de Chimie Pub Date : 2022-01-31 DOI:10.37358/rc.22.1.8498
Gang Li, Y. Wang, Fen-Dou Wang
{"title":"Preparation and Properties of Mg(OH)2 Whiskers by Ion Exchange Resin Method","authors":"Gang Li, Y. Wang, Fen-Dou Wang","doi":"10.37358/rc.22.1.8498","DOIUrl":null,"url":null,"abstract":"\nMg(OH)2 whiskers were successfully prepared under mechanical stirring with D301 ion exchange resin and Mg(NO3)2. The products were systematically characterized by testing settling ratio, turbidity, and analyzing SEM, FT-IR. The results showed that Mg(OH)2 prepared with 0.05 or 0.1 mol/L Mg(NO3)2 had excellent dispersion, and the settling ratio was close to 100 % after 360 min; The time extension was extremely helpful to improve the dispersion; The dispersion of product was correspondingly good under pH value of about 9. The products synthesized with different concentrations and reaction time could reach nanoscale, and the product obtained using 0.05 mol/L Mg(NO3)2 for 4 h had whisker structure with a length of 10 im and had a lipophilicity. FT-IR analysis showed the product included some functional groups or fragments from the resin, which had a positive modification effect on the products. The preparation of Mg(OH)2 whisker with resin as raw material is simple, green, and environmentally friendly, which is worthy of further application.\n","PeriodicalId":21296,"journal":{"name":"Revista de Chimie","volume":"48 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-01-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Revista de Chimie","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.37358/rc.22.1.8498","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"Materials Science","Score":null,"Total":0}
引用次数: 0

Abstract

Mg(OH)2 whiskers were successfully prepared under mechanical stirring with D301 ion exchange resin and Mg(NO3)2. The products were systematically characterized by testing settling ratio, turbidity, and analyzing SEM, FT-IR. The results showed that Mg(OH)2 prepared with 0.05 or 0.1 mol/L Mg(NO3)2 had excellent dispersion, and the settling ratio was close to 100 % after 360 min; The time extension was extremely helpful to improve the dispersion; The dispersion of product was correspondingly good under pH value of about 9. The products synthesized with different concentrations and reaction time could reach nanoscale, and the product obtained using 0.05 mol/L Mg(NO3)2 for 4 h had whisker structure with a length of 10 im and had a lipophilicity. FT-IR analysis showed the product included some functional groups or fragments from the resin, which had a positive modification effect on the products. The preparation of Mg(OH)2 whisker with resin as raw material is simple, green, and environmentally friendly, which is worthy of further application.
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
离子交换树脂法制备Mg(OH)2晶须及其性能
以D301离子交换树脂和硝酸镁为原料,在机械搅拌条件下成功制备了硝酸镁晶须。通过沉降比、浊度、扫描电镜(SEM)、红外光谱(FT-IR)分析对产物进行了系统表征。结果表明,以0.05或0.1 mol/L Mg(NO3)2制备的Mg(OH)2具有良好的分散性能,360 min后沉淀率接近100%;时间的延长对色散的改善有极大的帮助;在pH值约为9时,产物的分散性相应较好。不同浓度和反应时间合成的产物均可达到纳米级,在0.05 mol/L Mg(NO3)2条件下反应4 h得到的产物具有10 μ m长的晶须结构和亲脂性。FT-IR分析表明产物中含有树脂的官能团或片段,对产物有积极的改性作用。以树脂为原料制备Mg(OH)2晶须工艺简单、绿色环保,值得进一步推广应用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
Revista de Chimie
Revista de Chimie 化学-工程:化工
自引率
0.00%
发文量
54
审稿时长
3-6 weeks
期刊介绍: Revista de Chimie publishes original scientific studies submitted by romanian and foreign researchers and offers worldwide recognition of articles in many countries enabling their review in the publications of other researchers. Published articles are in various fields of research: * Chemistry * Petrochemistry * Chemical engineering * Process equipment * Biotechnology * Environment protection * Marketing & Management * Applications in medicine * Dental medicine * Pharmacy
期刊最新文献
Separation and Identification of Molecular Species by GC-MS for the Reaction Mixture with Methyltrimethoxysilane (MTMOS) Computational Structural Assessment on the Stereochemistry of the Transition Metal Complex Formed by a Naphthalene-1,4-dione Based Ligand with Divalent Nickel Analysis of Octane Retention Prediction Model for Catalytic Cracked Gasoline Based on Ridge Regression Model and Gradient Descent Optimization Separation and Identification of Molecular Species by GC-MS for the Reaction Mixture with Methyltrimethoxysilane (MTMOS) Computational Structural Assessment on the Stereochemistry of the Transition Metal Complex Formed by a Naphthalene-1,4-dione Based Ligand with Divalent Nickel
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1